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Grain boundary motion in aluminum bicrystals.

机译:铝双晶中的晶界运动。

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摘要

In this thesis, we studied the pure aluminum bicrystal system by giving the bicrystal specimens a moderate strain (10%--20%)individually on the Instron machine. The two grains were strained differently due to the different Schmid factor. The specimens were then annealed at 500°C in the furnace for a certain amount of time and cooled in the air. EBSD technique was used to track the grain boundary motion and triple junction formation during the annealing process after the specimens were electropolished.; We observed that various types of boundary motion occurred for different amount of strains. For specimens that were given 20% strain, stable triple junctions were observed at the end of the less-strained grain after a short period of time. In order to track the boundary migration, we strained two specimens for 10% and observed the whole boundary migration process during the aging. In another specimen that was strained 16%, multiple small grains was observed to appear in the more-strained grain at the early stage of annealing and we were able to trace the entire grain growth process.; Several important conclusions can be made after careful analysis on the results of above specimens. Strain-induced grain boundary migration (SIBM) was confirmed to be the dominant mechanism during the recrystallization and the subsequent grain growth and the migration rate could be proportional to the strain energy stored in the adjacent grains. For the specimen that formed a number of small grains in the annealing process, we noticed that the proportion of CSL special boundaries was not changed significantly during annealing, which means gain growth might not be an effective way to increase the number of CSL boundaries in aluminum. Also, study on the grain boundary triple junctions in this specimen showed that the shape of a triple junction was largely affected by the boundary energy of its components.
机译:在本文中,我们通过在Instron机器上分别给双晶试样分别施加中等应变(10%-20%)来研究纯铝双晶体系。由于不同的施密特因子,两种晶粒的应变不同。然后将样品在炉中于500°C退火一定时间,然后在空气中冷却。 EBSD技术用于跟踪样品电抛光后退火过程中的晶界运动和三重结形成。我们观察到,不同数量的应变会发生各种类型的边界运动。对于应变为20%的试样,在短时间后,在应变较小的晶粒末端观察到稳定的三重结。为了跟踪边界迁移,我们将两个样本应变为10%,并观察了老化过程中的整个边界迁移过程。在另一个应变为16%的试样中,观察到在退火的早期阶段,应变较大的晶粒中出现了多个小晶粒,并且我们能够追踪整个晶粒的生长过程。通过仔细分析上述标本的结果,可以得出几个重要的结论。应变诱导的晶界迁移(SIBM)被证实是重结晶过程中的主要机制,随后的晶粒长大和迁移速率可能与相邻晶粒中存储的应变能成正比。对于在退火过程中形成许多小晶粒的试样,我们注意到CSL特殊边界的比例在退火过程中没有显着变化,这意味着增益增长可能不是增加铝中CSL边界数量的有效方法。 。另外,对该样品的晶界三重结的研究表明,三重结的形状在很大程度上受到其组分的边界能的影响。

著录项

  • 作者

    Xiao, Guanghao.;

  • 作者单位

    Brown University.;

  • 授予单位 Brown University.;
  • 学科 Engineering Materials Science.
  • 学位 Ph.D.
  • 年度 2005
  • 页码 99 p.
  • 总页数 99
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类 工程材料学;
  • 关键词

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