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CHARACTERIZATION OF SILICON FUSION BONDS USING A FOUR-POINT BEND SPECIMEN

机译:用四点弯曲试样表征硅熔合键

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The increased number of MEMS devices that are fabricated by bonding two or more bulk micromachined silicon wafers has highlighted the need to produce reliable silicon fusion bonds. The current study focuses on employing a four-point bend delamination specimen to measure silicon fusion bond strength as a function of processing conditions. The specimen, which is composed of two bonded layers and an initial notch, permits the measurement of a mixed-mode critical strain energy rate, Gc, at the interface. This specimen geometry is advantageous because it does not require measurement of crack length to calculate the strain energy release rate and is insensitive to damage near the specimen edges. The fact that the interface is loaded under mixed-mode conditions presents difficulties in achieving stable crack propagation in well bonded specimens. Attempts were made to eliminate this problem by reducing the effective bond toughness by etching shallow grooves in the wafer surfaces to reduce the bonded area. Testing revealed that while this approach reduced the effective toughness of the interface, it did not prevent crack deflection in well bonded samples. Despite the limitations of the specimen, data was obtained for silicon fusion bonds fabricated under various annealing and contacting conditions. Test results indicate an increase in bond toughness with annealing temperature and time. The data also suggests that the contacting pressure and duration have little effect on bond quality. The specimen, while limited to characterizing bonds with lower toughness, proved straightforward to fabricate and test.
机译:通过键合两个或更多个块状微机械加工的硅晶片而制造的MEMS器件数量的增加,凸显了对生产可靠的硅熔合键的需求。当前的研究集中在采用四点弯曲分层试样来测量硅熔融粘合强度作为加工条件的函数。由两个粘结层和一个初始槽口组成的样品允许在界面处测量混合模式的临界应变能速率Gc。这种样品几何形状是有利的,因为它不需要测量裂纹长度即可计算应变能释放速率,并且对样品边缘附近的损坏不敏感。在混合模式条件下加载界面的事实为在粘结良好的试样中实现稳定的裂纹扩展提供了困难。尝试通过在晶片表面刻蚀浅槽以减小粘结面积来降低有效粘结韧性来消除该问题。测试表明,尽管这种方法降低了界面的有效韧性,但并不能防止粘结良好的样品出现裂纹变形。尽管样品有局限性,但仍获得了在各种退火和接触条件下制造的硅熔合数据的数据。测试结果表明,粘合韧性随退火温度和时间的增加而增加。数据还表明接触压力和持续时间对粘结质量影响很小。该样品虽然仅限于表征具有较低韧性的粘结,但事实证明,它易于制造和测试。

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