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Properties Of Calcium Phosphate Thin Film Biomaterials With The Addition Of Titanium Oxide

机译:氧化钛氧化钛磷酸钙薄膜生物材料的性质

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Thin films were synthesized by sol-gel method from alcohol film forming solutions (FFS) based on tetraethoxysilane, phosphoric acid, calcium chloride. Concentration of tetrabutoxytitanium was 0.4 and 0.3 M. Thin films were produced on substrates of single crystal silicon (model substrate) by spin-coating with a centrifuge speed of 3000 rev/min, followed by heat treatment at 60 °C for 20 minutes and at 600 °C for 1 h. During the experiment it was found that film with uniform surface may be got on the fifth day after preparation of the solution with a concentration of Ti~(4+) 0.3 M. For homogeneous material requires heat treatment at 800 °C. The highest bioactivity was observed in the films based on film-forming solution with a concentration of Ti~(4+) 0.3 M.
机译:通过基于四乙氧基硅烷,磷酸,氯化钙的醇膜形成溶液(FF)通过溶胶 - 凝胶法合成薄膜。 通过旋涂在单晶硅(模型基材)的基板上产生薄膜,在单晶硅(模型基材)的基板上,通过旋转速度为3000°/ min,然后在60℃下热处理20分钟,然后在60℃下进行薄膜20分钟 600°C为1小时。 在实验期间,发现具有均匀表面的薄膜可以在制备溶液的浓度为Ti〜(4+)0.3M后的第五天。对于均匀材料需要在800℃下热处理。 基于薄膜在薄膜中观察到最高的生物活性,其成膜溶液具有Ti〜(4+)0.3米的浓度。

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