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Dynamic measurement of reflectance/emissivity in mid-infrared band

机译:中红外频段反射/发射率的动态测量

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In order to measure the change of laser energy coupling coefficient with temperature in mid-infrared wave band, reflectance integrating sphere experiment system was designed and set up. 915nm CW laser was used to heat samples and the wavelength of probe laser is 3.8μm. Chopper and phase-locked amplifier were adopted in the system. Thermal imager was used to measure and record the temperature of samples during laser irradiation. The reflectance of steel and aluminum plates to 3.8μm was measured during 915nm laser irradiation. EDS analysis was done to investigate the change of elemental composition in the samples respectively. The experimental results show that, the results of reflectance and radiation temperature measured by this system are relatively accurate during laser irradiation. In the process of temperature rising from 300K to 785K, the color of 45# steel plates turns blue and black, while the color of aluminum alloy plates is basically unchanged. When temperature reaches about 700K, reflectance of 45# steel decreases obviously with the increase of temperature, while reflectance of aluminum is almost constant. The reflectance is probably determined by the oxide in the surface of samples which is consistent with the results of EDS analysis. Reflectance decreases with the increase of the content of oxygen in the surface. The reason of why the reflectance of aluminum is almost constant is that aluminum oxide is not generate massively under 750K.
机译:为了测量中红外波段温度的激光能量耦合系数的变化,设计并建立了反射集成球实验系统。 915NM CW激光用于加热样品,探针激光的波长为3.8μm。在系统中采用斩波器和锁相放大器。热成像仪用于测量并记录激光照射期间样品的温度。在915nm激光照射期间测量钢和铝板的反射率至3.8μm。进行EDS分析以分别研究样品中元素组成的变化。实验结果表明,在激光照射期间,该系统测量的反射率和辐射温度的结果相对准确。在温度下升到300k至785k的过程中,45#钢板的颜色变为蓝色和黑色,而铝合金板的颜色基本不变。当温度达到700K大约700K时,45#钢的反射率随着温度的增加而显然降低,而铝的反射率几乎是恒定的。反射率可能由样品表面中的氧化物确定,这与EDS分析的结果一致。随着表面氧含量的增加,反射率降低。为什么铝的反射率几乎是恒定的,即氧化铝不会在750K下产生大量的。

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