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Transient liquid phase bonding of alumina to alumina via Bismuth oxide interlayer

机译:氧化铋层间氧化铝至氧化铝的瞬态液相结合

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Bismuth oxide, due to its low melting point was selected as filler for joining alumina to alumina using Transient Liquid Phase (TLP) method. For this purpose a thin layer of bismuth oxide was placed as an interlayer between the ceramic bodies. To study the effect of time and temperature on the mechanical properties of the joined samples, the joining tests were carried out in 900, 1000 and 1100°C for various times. The mechanical properties of the joined samples were measured using shear testing method. To investigate the microstructure of the joining area, the cross section ofthe joints were studied using scanning electron microscope (SEM) and X-ray diffraction method. The results showed that longer joining times results in higher mechanical properties of the joints. The highest joint strength of about 80MPa was obtained for the sample joined in 900°C for lOhour.
机译:氧化铋,由于其低熔点,选择使用瞬时液相(TLP)方法将氧化铝与氧化铝连接到氧化铝的填料。为此目的,将薄薄的氧化铋层作为陶瓷体之间的中间层置于夹层中。为了研究时间和温度对连接样品的力学性能的影响,将连接试验在900,1000和1100℃下进行各个时间。使用剪切测试方法测量接合样品的机械性能。为了研究连接区域的微观结构,使用扫描电子显微镜(SEM)和X射线衍射方法研究了关节的横截面。结果表明,较长的接合时间导致关节的较高机械性能。获得在900℃的样品中获得约80MPa的最高关节强度,用于LOHOUR。

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