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Effect of Nickel Catalyst on Carbon Nanotubes by using Palm Oil as a Starting Material

机译:用棕榈油作为原料碳纳米管镍催化剂对碳纳米管的影响

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Carbon nanotubes (CNTs) were produced on silicon (Si) substrate prepared by Thermal-CVD method using C_(55)H_(96)O_6 (Palm Oil) as a starting material. Catalyst has been prepared by dissolving Nickel (II) nitrate, Ni (NO_3)_2-6H_2O and ethyl alcohol, C_5H_5OH. The CNTs was deposited on nickel coated silicon where the nickel acts as catalyst .Various parameters such as amount of catalyst, amount of palm oil, deposition time, deposition temperature, flow rate of gas and carrier gas have been studied. By using Thermal-CVD, samples were penetrated using NH_3 (argon) gas at a temperature 700-900°C for catalyst and 450°C for Palm Oil. Surface morphology and uniformity of CNTs were characterized using FESEM at different deposition temperature. Chemical functional groups of CNTs were characterized using FTIR. The surface morphology and uniformity of CNTs are dependents on parameters used.
机译:在使用C_(55)H_(96)O_6(棕榈油)作为起始材料的热CVD方法制备的硅(Si)底物上产生碳纳米管(CNT)。催化剂已经通过溶解镍(II)硝酸镍,Ni(NO_3)_2-6H_2O和乙醇,C_5H_5OH来制备。 CNT沉积在镍涂覆的硅上,其中镍用作催化剂。已经研究了催化剂的量,例如催化剂量,棕榈油量,沉积时间,沉积温度,气体和载气的流速。通过使用热CVD,使用NH_3(氩气)在700-900℃的温度下进行样品,用于催化剂和450℃的棕榈油。在不同沉积温度下使用FESEM表征CNT的表面形态和均匀性。使用FTIR表征CNT的化学官能团。 CNT的表面形态和均匀性是对所用参数的基因。

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