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Aluminizing Coating Prepared on Oil Casing Steel N80 by Low-Temperature Pack Cementation

机译:通过低温包装胶结在油套管钢N80上制备铝化涂料

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Aluminizing has been verified to be an effective way to improve the corrosion resistance of steel due to the formation of continuous Al_2O_3 layer, but traditional aluminizing processing carried out at high temperature can not be used to prepare aluminide layer on the surface of oil casing steel. In this paper, an aluminide coating was prepared on oil casing steel N80 by a low-temperature pack cementation only at 803 K for 2 hours by adding zinc in the pack powder and pre-treatment of N80 substrate by surface mechanical attrition. The phase composition, microstructure, element distribution and properties of as-aluminized oil casing steel N80 were characterized by means of XRD, SEM, EDS, micro-hardness test and electrochemical corrosion measurements. The results indicate that aluminide coating mainly consists of FeAl_3, Fe_2Al_5 and FeAl. The continuous aluminide coating with an average thickness around 50 ìm could be successfully formed on the surface of oil casing steel N80 which shows a good coherence with as-packed substrate. After preparation of aluminide coating, oil casing steel N80 shows a higher microhardness in the range of aluminizing coating than that of the virgin material because of the formation of iron aluminide. The exception noted is that the proposed low-temperature aluminizing processing does not have any damaging impact on the mechanical properties of steel substrates. Moreover, it is concluded that oil casing steel N80 with aluminizing coating shows a better corrosion resistance than that of original N80 by analyzing of electrochemical test results.
机译:铝化已经被验证为提高钢耐腐蚀性导致钢的耐腐蚀性的有效方法,但在高温下进行的传统铝化加工不能用于在油套管表面上制备铝化层。本文通过在803k下,通过在包装粉末中加入锌,在803k下,在油壳壳钢N80上制备铝化物涂层,并通过表面机械磨损预处理N80底物。通过XRD,SEM,EDS,微硬度测试和电化学腐蚀测量来表征AS铝制油套管钢N80的相组合物,微观结构,元件分布和性能。结果表明,铝化涂层主要由FEAL_3,FE_2AL_5和FEAL组成。在油壳钢N80的表面上可以成功形成具有平均厚度约50μm的连续铝化涂层,其显示出与用填充基板的良好相干性。在制备铝化涂层后,由于铁铝化物的形成,油壳钢N80在铝化涂层的范围内显示出更高的微硬度,而不是原子材料。例外指出的是,所提出的低温铝化加工对钢基材的机械性能没有任何损害影响。此外,结论是通过分析电化学测试结果,具有铝化涂层的油套管钢N80显示出比原始N80更好的耐腐蚀性。

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