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Study of the Thermal Stability and Structural Featuresin Nanostructured Aluminum 2024 Alloy Obtained by Cryomilling

机译:纳米结构铝2024合金的热稳定性和结构特征研究

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In the present work, the nanostructured aluminum 2024 alloy produced by cryomilling and consolidated by Spark Plasma Sintering (SPS) was investigated. The powder milled in liquid nitrogen shows a distribution of the particle size, ranging between few microns up to about 90 μm.The granulometric classes selected are <25 μm, 25-45 μm, 45-90 μm. For each granulometric classes, the structural and the microstructural features, as well as the transformations involving coherent precipitates (AI-2Cu and AI-2CuMg) and thermal stability were investigated. The analyses are done using X-ray diffraction. The interest on these transformations arises from the awareness that the thermal stability of the nanostructured powder requires a sintering temperature close to 500°C to obtain a full dense material. This effect of the nanostructure on these transformations was investigated.
机译:在本作工作中,研究了通过冷冻血浆烧结(SPS)而通过冷冻和固结的纳米结构铝2024合金。在液氮中研磨的粉末显示出粒度的分布,范围为少于约90μm。选择的粒度等级为<25μm,25-45μm,45-90μm。针对每个粒状类,研究结构和微观结构特征以及涉及相干沉淀物(AI-2CU和AI-2cumG)和热稳定性的变化。通过X射线衍射进行分析。这些转化的兴趣引起了意识,即纳米结构粉末的热稳定性需要接近500℃的烧结温度以获得全致密材料。研究了纳米结构对这些转化的这种效果。

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