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Fabrication of Nanostructured, Submicronic Metal Powders by Double Ultrasonic Atomisation

机译:双超声雾化制备纳米结构,亚微晶金属粉末的制备

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An atomiser is designed for the production of nanostructured, submicronic metal powders with melting points up to 2000°C. The alloy is induction-melted in a vacuum and subsequently argon-stirred for homogenisation. The break-up of the superheated melt into spherical droplets is carried out in a tubular ultrasonic resonator under argon or helium atmosphere. Droplet size is governed by the ultrasonic parameters of newly developed transducers. Rapid solidification of the atomised melt is the result of convective cooling. For the controlled passivation of the solidified droplets, a mixture of oxygen and carbon dioxide is added to the gas flowing inside the atomising vessel. Once optimised, this method is expected to be commercially viable for the production of special powders in small batches for advanced powder technology processing.
机译:雾化器设计用于生产纳米结构,亚微型金属粉末,熔化点高达2000℃。合金在真空中诱导熔化,随后搅拌均匀化。在氩气或氦气气氛下的管状超声谐振器中,将过热熔体分解成球形液滴。液滴尺寸由新开发的传感器的超声波参数控制。雾化熔体的快速凝固是对流冷却的结果。对于固化液滴的受控钝化,将氧和二氧化碳的混合物加入到雾化容器内流动的气体中。优化后,该方法预计将在用于高级粉末技术加工的小批次中生产特殊粉末的商业可行性。

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