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Cancelling energy drift in a PEELS spectrometer

机译:取消剥离光谱仪的能量漂移

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摘要

The possible spectral resolution in parallel-recorded electron energy-loss spectroscopy (PEELS) attained with a STEM is nearing the fundamental limit set by the energy spread of its cold field-emission electron gun (approx. 0.25 eV). The stabilities of the power supplies (high voltage and bending magnet current) are the main obstacles to realising this resolution: about 1 ppm must be maintained during the exposure. This paper describes a method that fixes the position of the zero-loss peak so that it is not affected by power supply drift; some examples of energy-loss spectra are included.
机译:具有杆的并联记录的电子能损光谱(皮带)中的可能的光谱分辨率接近其冷场 - 发射电子枪(约0.25eV)的能量扩展设定的基本限制。电源(高电压和弯曲磁电流)的稳定性是实现该分辨率的主要障碍:在曝光期间必须保持约1ppm。本文介绍了一种修复零损耗峰值的方法,使其不受电源漂移的影响;包括能量损耗光谱的一些示例。

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