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The origin of particle (oxide) traces in friction stir welds

机译:摩擦搅拌焊缝中颗粒(氧化物)痕量的起源

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Since the invention of FSW many publications mentioned the particular stirred zone features (onion ring like structure) of FSW joints, which is caused by material flow and deformation and subsequent recrystallization. Beside this artefact there are sometimes line peculiarities in the joint that do not follow the onion ring type structure. Especially AlMgSi (6xxx type) alloys seem to be preferred to create these particle rows which prove to be micro meter sized fragments during high resolution, metallurgical investigation aligned in the bulk material. First investigations using SEM and EDX indicated that these phases might be aluminium and magnesium oxides. However the amount of particles that can be found is unexpected high compared to the known natural oxide layer thickness on standard Al materials (before joint by FSW). Additionally premature joint failures are sometimes linked with this very specific weld seam contamination. A fundamental investigation had been performed using and characterising ultra clean Al (99.999 percent), standard Al (99.5 percent) and an AlSiMgCu alloy (AA 6056). Three different surface preparations were applied prior FSW processing combined with 2 different FSW tool geometries. Detailed metallurgical and scanning electron examination were conducted to create a basic understanding of origin and interaction of the oxide contaminations that were detected in the welds. One focus was put to the question whether the oxide particles and their amount are determined prior to welding or an "in situ" generation of oxides during welding might occur.
机译:由于FSW的发明许多出版物提到了FSW接头的特定搅拌区特征(洋葱环状结构),这是由材料流动和变形和随后的再结晶引起的。除此之外,有时在接头中有时不遵循洋葱环型结构。特别是Almgsi(6xxx型)合金似乎是优选的,以产生这些粒子行,该颗粒行被证明在高分辨率期间是微米尺寸的碎片,在散装材料中对齐的冶金研究。使用SEM和EDX的首次研究表明这些相可能是铝和氧化镁。然而,与标准Al材料上的已知的自然氧化物层厚度相比,可以发现的颗粒的量是出乎意料的高(在FSW之前)。另外过早的关节故障有时与这种非常特定的焊缝污染有关。使用和表征超清洁Al(99.999%),标准Al(99.5%)和Alsimgcu合金(AA 6056)进行了基础调查。应用了三种不同的表面制剂,先前的FSW加工结合了2种不同的FSW工具几何形状。进行了详细的冶金和扫描电子检查以创造对焊缝中检测到的氧化物污染的原始和相互作用的基本理解。对氧化物颗粒及其量在焊接之前确定氧化物颗粒及其量的问题,可能发生一个焦点,或者可能发生焊接期间的“原位”产生氧化物的“原位”。

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