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NEW NIST MERCURY TRIPLE-POINT CELLS

机译:新的NIST水星三重点细胞

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Six new Hg triple-point (TP) cells (234.3156 K) were manufactured in the NIST PRT Laboratory for use in the realization of the International Temperature Scale of 1990 (ITS-90). The fixed-point cells consisted of both glass and stainless steel designs with either an 8 mm or 12 mm inner diameter reentrant well. Triple-distilled Hg with nominal purities of 99.999 999 wt.% were used to fill the cells using a vacuum distillation filling process. The certification method of the new cells included measuring melting curve plateaus, direct comparisons with the PRT Laboratory reference Hg TP cell (Hg SS-1), and immersion profiling. The estimated amount of impurities leached out of the stainless steel crucible into the Hg sample of Hg SS-1 over 25 years was found to be 1 μg/g. This paper presents the fixed-point cell designs, fabrication method, results from the cell certification procedures, and the estimated uncertainty assigned to the Hg TP cells.
机译:在NIST PRT实验室中制造了六个新的HG三点(TP)细胞(234.3156 k),以实现1990年的国际温度等级(其-90)。固定点电池由玻璃和不锈钢设计的固定点电池包括8mm或12mm的内径倒回良好。具有99.999 999重量%的标称纯度的三蒸馏Hg。使用真空蒸馏填充过程来填充细胞。新细胞的认证方法包括测量熔化曲线平台,与PRT实验室参考HG TP细胞(Hg SS-1)的直接比较和浸入性分​​析。将含量浸出的含有不锈钢坩埚的估计量为Hg SS-1超过25年的Hg SS-1的样品为1μg/ g。本文介绍了固定点电池设计,制造方法,来自小区认证程序的结果,以及分配给HG TP细胞的估计不确定性。

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