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System for in-situ dielectric and calorimetric measurements during microwave curing of resins

机译:用于树脂微波固化过程中的原位介电和量热测量系统

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The use of new materials is of great interest for science, research and industry. Fiber composite materials such as carbon fiber or glass fiber composites find due to their lightweight potential, as well as their mechanical and physical features increasing application in aerospace engineering, the automotive industry and the general engineering. The main obstacle to these materials is the difficulty of manufacturing with long cycle times and high energy consumption. Therefore, it is of great interest to find new approaches, which accelerate the production of fiber composites, while making it more energy-efficient. Here, the microwave curing is a promising technology for the preparation of fiber-reinforced composites, as it is faster and more cost-effective, because it is based on the volumetric heating of the material. This motivated the development of various microwave systems and processes. Nevertheless, for a successful system and process design the detailed knowledge of the dielectric properties of materials is mandatory. Therefore, a system for in-situ monitoring of curing processes of thermoset resins under microwave heating was developed. The main function of the measurements instrument is the dielectric characterization of resins based on the cavity perturbation technique. Here, the electromagnetic source used for dielectric characterization of the material under test is used for dielectric heating at the same time. The cavity operates at 2.45 GHz in the TE mode. It has an unloaded quality factor of 11500. In addition, a calorimetric analysis of the exothermal curing process is envisaged.
机译:新材料的使用对科学,研究和工业具有极大的兴趣。诸如碳纤维或玻璃纤维复合材料之类的纤维复合材料因其轻量化的潜力以及其机械和物理特性而日益广泛地应用在航空航天工程,汽车工业和通用工程中。这些材料的主要障碍是制造难度大,周期时间长,能耗高。因此,寻找新的方法非常感兴趣,这些方法可以加速纤维复合材料的生产,同时使其更加节能。在此,微波固化是一种制备纤维增强复合材料的有前途的技术,因为它基于材料的体积加热,因此速度更快且更具成本效益。这激发了各种微波系统和工艺的发展。然而,对于成功的系统和工艺设计,必须具有对材料介电性能的详细了解。因此,开发了一种在微波加热下原位监测热固性树脂固化过程的系统。测量仪器的主要功能是基于腔扰动技术对树脂进行介电表征。在此,用于测试材料介电特性的电磁源同时用于介电加热。腔在TE模式下的工作频率为2.45 GHz。它的空载质量因数为11500。此外,还设想了放热固化过程的量热分析。

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