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MECHANICAL BEHAVIOUR AND MICROSTRUCTURE CORRELATION IN A SELECTIVE LASER MELTED SUPERALLOY

机译:选择性激光熔炼高温合金的力学行为和微观结构相关性

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Selective laser melting (SLM), or, as the industry standard denotes the process, laser sintering, is an additive manufacturing process where metal powder is melted by a laser source layer-wise, forming a solid, dense metallic component. With the SLM process, near net shape components can be manufactured directly from a CAD model. The model is sliced into thin (max 100μm thick) layers. Powder is spread onto a metallic build platform and the powder is fused by a laser as dictated by the CAD model. The laser energy is intense enough to permit full melting (welding) of the particles to form solid metal. The process is repeated layer by layer until the part is complete. A number of materials are available, including steel, aluminium, titanium and, in recent time, also superalloys. The material investigated in the current project is an alloy in agreement with the composition of Haynes International Hastelloy X, a solution strengthened superalloy typically used in large welded components exposed to high temperatures in oxidizing as well as reducing environments. Microstructurally, the material is different from both a hot-rolled, as well as a cast material due to the manufacturing process. Since the SLM process involves laser melting of powder particles in the size range of <50μm, the structure resembles of a weld structure, however on a smaller scale. Due to the layer-by-layer build strategy, the material will exhibit anisotropy. Different heat treatment approaches can be adopted in order to homogenize the material and to minimize the effect of anisotropy. A stress relieve heat treatment was adopted and compared to the findings of the as manufactured SLM material. The current project focuses on evaluating mechanical properties for a material manufactured by the SLM process and comparing to data for established manufacturing processes. For evaluation of the mechanical properties, low cycle fatigue testing and tensile testing has been performed. The microstructure and material deformation / cracking are evaluated by light optical microscopy and SEM, where electron backscatter diffraction is used. Due to the weld-like structure, the material will be transversely isotropic in the as-manufactured condition with one symmetry plane perpendicular to the build direction. Any direction perpendicular to the build direction tends to give increased strength compared to a direction parallel to the build direction if monotonic data are concerned. If fatigue properties are concerned, the anisotropy is also obvious. It is shown that the differences in behaviour can be coupled to microstructure.
机译:选择性激光熔化(SLM)或作为行业标准所表示的过程,即激光烧结,是一种增材制造过程,其中,金属粉末通过激光源逐层熔化,形成固体致密的金属成分。通过SLM工艺,可以直接从CAD模型中制造出接近最终形状的零件。将模型切成薄层(最大100μm厚)。将粉末散布到金属成型平台上,然后按照CAD模型的指示,通过激光将粉末熔化。激光能量足够强,可以使颗粒完全熔化(焊接)以形成固体金属。逐层重复此过程,直到完成零件。有许多材料可供使用,包括钢,铝,钛以及最近的高温合金。当前项目中研究的材料是与Haynes International Hastelloy X的成分一致的合金,这是一种溶液增强的高温合金,通常用于暴露于氧化和还原环境中高温的大型焊接部件。在微观结构上,由于制造工艺的原因,该材料既不同于热轧材料,也不同于铸造材料。由于SLM工艺涉及激光熔化尺寸小于50μm的粉末颗粒,因此该结构类似于焊接结构,但是规模较小。由于逐层构建策略,该材料将表现出各向异性。为了使材料均匀并且最小化各向异性的影响,可以采用不同的热处理方法。采用了应力消除热处理,并将其与制成的SLM材料的发现进行了比较。当前项目的重点是评估通过SLM工艺制造的材料的机械性能,并与已建立的制造工艺的数据进行比较。为了评估机械性能,已进行了低周疲劳测试和拉伸测试。微观结构和材料变形/开裂通过光学显微镜和SEM进行评估,其中使用了电子背散射衍射。由于具有类似焊缝的结构,材料在制造状态下将具有横向各向同性的特性,其中一个对称平面垂直于构建方向。如果涉及单调数据,则与平行于构建方向的方向相比,任何垂直于构建方向的方向都倾向于增加强度。如果考虑疲劳性能,则各向异性也很明显。结果表明,行为差异可以与微观结构耦合。

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