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Optical characterization of anti reflective sol-gel coatings fabricated using dip coating method

机译:使用浸涂法制备的抗反射溶胶-凝胶涂层的光学特性

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laser induced damage; sol-gel; anti-reflective coating; dip coating; colloidal silica nanoparticlesIn recent years, there has been a growing interest in further development of sol-gel method which can produce ceramics and glasses using chemical precursors at relative low-temperatures. The applications for sol-gel derived products are numerous. Department of General and Inorganic Chemistry with Laser Research Center of Vilnius University and Institute of Physics continues an ongoing research effort on the synthesis, deposition and characterization of porous sol-gel. Our target is highly optically resistant anti-reflective (AR) coatings for general optics and nonlinear optical crystals. In order to produce AR coatings a silica (SiO_2) sol-gel has been dip coated on the set of fused silica substrates. The optical properties and structure of AR-coatings deposited from hydrolysed tetraethylorthosilicate (TEOS) sol were characterized in detail in this study. The influence of different parameters on the formation of colloidal silica antireflective coatings by dip-coating technique has been investigated. All samples were characterized performing, transmission electron microscopy, UV-visible spectroscopy, atomic force microscopy, ellipsometric, total scattering and laser-induced damage threshold measurements. Herewith we present our recent results on synthesis of sol-gel solvents, coating fabrication and characterization of their optical properties.
机译:激光引起的损坏;溶胶凝胶防反射涂层;浸涂胶体二氧化硅纳米粒子 近年来,人们对溶胶-凝胶法的进一步发展越来越感兴趣,该方法可以在相对低温下使用化学前体生产陶瓷和玻璃。溶胶-凝胶衍生产品的应用非常广泛。维尔纽斯大学激光研究中心和物理研究所的普通和无机化学系继续进行多孔溶胶-凝胶的合成,沉积和表征研究。我们的目标是为普通光学器件和非线性光学晶体提供高光学抗反射(AR)涂层。为了生产增透膜,已将二氧化硅(SiO_2)溶胶-凝胶浸涂在这组熔融的二氧化硅基材上。在这项研究中,详细描述了由水解原硅酸四乙酯(TEOS)溶胶沉积的增透膜的光学性质和结构。研究了不同参数对浸涂技术形成胶体二氧化硅减反射膜的影响。所有样品均进行了性能表征,透射电子显微镜,紫外可见光谱,原子力显微镜,椭圆光度法,总散射和激光诱导的损伤阈值测量。因此,我们提出了关于溶胶-凝胶溶剂合成,涂层制备及其光学特性表征的最新研究成果。

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