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Change in the microstructure and mechanical properties of drawn pearlitic steel with low-temperature aging

机译:低温时效拉伸珠光体钢的组织和力学性能变化

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Hydrogen embrittlement is a serious problem in high-strength steels. Drawn pearlitic steel shows excellent resistance to hydrogen embrittlement despite its high strength, and aging treatment at a low temperature can simultaneously improve its strength and hydrogen-embrittlement resistance. To clarify the mechanism for this we have used thermal desorption analysis (TDA) and the newly developed precession electron diffraction analysis method in the transmission electron microscope. After agingat 100 °C for 10 min, the amount of hydrogen seen amount on the TDA curve reduced at around 100 °C. In contrast, when aging was performed at 300 °C, the hydrogen amount further reduced at around 100 °C and the unevenly deformed lamellar ferrite zone was locally recovered. For the samples that were aged at the low temperature, we confirmed that their yield strength and relaxation stress ratios increased simultaneously with improvement in the hydrogen-embrittlement property. We infer that segregation of carbon or formation of very fine carbide in dislocations during aging is the cause of these behaviors.
机译:氢脆是高强度钢中的一个严重问题。拉丝珠光体钢尽管强度高,但仍表现出优异的抗氢脆性,而低温时效处理可同时提高强度和抗氢脆性。为了阐明其机理,我们在透射电子显微镜中使用了热脱附分析(TDA)和最新开发的旋进电子衍射分析方法。在100°C下老化10分钟后,TDA曲线上可见的氢气量在100°C左右减少。相反,当在300℃下进行时效时,在100℃附近氢量进一步减少,并且局部恢复了不均匀变形的层状铁素体区。对于在低温下老化的样品,我们确认了它们的屈服强度和弛豫应力比与氢包裹性的改善同时增加。我们推断,在时效过程中位错中碳的偏析或非常细小的碳化物的形成是这些行为的原因。

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