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Influence of Annealing on Strength of Ultrafine Grained Low Carbon Steels by ECAP

机译:ECAP退火对超细晶低碳钢强度的影响

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In the present study, ultra fine-grained low carbon steel samples were processed by equal channel angular pressing (ECAP). Mechanical properties of the specimens annealed statically at several temperatures were evaluated by tensile and hardness test. In addition, grain sizes of the specimens were measured by SEM-electron back scattering pattern (SEM-EBSP) and X-ray diffraction analysis. Differential scanning calorimetry (DSC) measurement also evaluated thermal reactions in anneal process of the specimen. As a result, the grain size was changed at the temperature between 550°C and 600°C drastically and the tensile strength also became lower at the same temperature. The relation between yield stress and averaged grain diameter of specimens obeyed the Hall-Petch relation except the normalized specimen. Behavior of grain growth and recovery in structural observation by EBSP corresponded to reaction signal of the DSC curve.
机译:在本研究中,超细晶粒低碳钢样品通过等通道角挤压(ECAP)进行了处理。通过拉伸和硬度测试评估在几个温度下静态退火的试样的机械性能。另外,通过SEM电子反向散射图案(SEM-EBSP)和X射线衍射分析来测量样品的晶粒尺寸。差示扫描量热法(DSC)测量还评估了样品退火过程中的热反应。结果,在550℃和600℃之间的温度下晶粒尺寸急剧变化,并且在相同温度下抗拉强度也降低。试样的屈服应力与平均粒径之间的关系除归一化试样外,均服从霍尔-帕奇关系。通过EBSP观察到的晶粒长大和恢复行为与DSC曲线的反应信号相对应。

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