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STUDIES ON TEXTURE AND MICROSTRUCTURE OF CRYOROLLED AND ANNEALED Cu-5Al, Cu-5Zn ALLOYS

机译:低温和退火Cu-5%Al,Cu-5%Zn合金的组织和显微组织研究

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In the present work, we report the crystallographic texture, microstructure and elastic modulus in Cu-5 wt. % Al and Cu-5 wt. % Zn alloys after cryorolling (true strain of e ~ 2) and annealing. Texture was studied using X-ray diffraction and electron back scatter diffraction in the scanning electron microscope. Cu-Al and Cu-Zn alloys were found to develop a strong texture after cryorolling and the texture weakens considerably following annealing in the range of 250-300°C. In-situ Young's modulus (E) measurements (using resonance technique) at temperatures from 25-300°C revealed that E is lowest in both the alloys (108-112 GPa) in the as-rolled condition and recovers to the isotropic value (128 GPa) after heating to 250-300°C. This could be correlated to the rolling and annealing textures in both the alloys. After annealing at 250°C for 15 min, a recrystallized ultra fine grained microstructure with an average grain size in the range of 0.5-1 μm with very fine twins was obtained in both the alloys. The grain boundary character distribution revealed significant fraction of CSL boundaries in both the alloys.
机译:在目前的工作中,我们报告了Cu-5 wt.g中的晶体织构,微观结构和弹性模量。 Al和Cu-5重量%。 %Zn合金经过冷轧(e〜2的真实应变)并退火后。在扫描电子显微镜中使用X射线衍射和电子背散射衍射研究了织构。发现Cu-Al和Cu-Zn合金在冷轧后会形成很强的织构,并且在250-300°C的温度范围内退火后,织构会明显减弱。在25-300°C的温度下(使用共振技术)测量原位杨氏模量(E),发现在轧制条件下,两种合金(108-112 GPa)中的E最低,并恢复到各向同性值(加热至250-300°C后,则为128 GPa)。这可能与两种合金的轧制和退火织构有关。在250°C退火15分钟后,在两种合金中均获得了重结晶的超细晶粒组织,其平均晶粒度在0.5-1μm范围内,并具有非常细的孪晶。晶界特征分布揭示了两种合金中都有很大一部分的CSL晶界。

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