A quartz-crystal-sensor oscillator appropriate for highly viscous liquid measurements

摘要

This paper describes a sensor oscillator appropriate for quartz crystal microbalance (QCM) based measurements in highly viscous liquids. The oscillator is stabilized by a recently developed impedance transformation QCM filter network which greatly reduces electrical load by the sustaining amplifier. In addition, it provides 0 phase and a well behaved symmetric resonance at the QCM series resonant frequency fs over three orders of magnitude variation range of the motional resistance Rm. The sustaining amplifier has a constant pure resistive input and output impedance to eliminate phase shifts due to QCM impedance changes with liquid load. Also it allows precise gain and phase control for accurate adjustment of the oscillator frequency at fs and extraction of Rm information at the measured liquid load. The oscillator was tested with different water based glycerol solutions in the 40wt% to 100wt% range. The worstcase frequency error was within 5% in this viscosity range.