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Numerical and experimental study of the circular cracks observed at the contact edges of the indentations of coated systems with soft substrates

机译:带有软质基材的涂层体系的压痕接触边缘处观察到的圆形裂纹的数值和实验研究

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In this work, the finite element method (FEM) was used, in conjunction with experiments, to study some of the crack patterns observed during the indentation of coated systems. In particular, the study was centered on the array of circular cracks observed close to the contact edge of the spherical indentations of systems with soft substrates. A sequence of steps was considered during the FEM formulation. Initially, the deposition (intrinsic) and thermal (extrinsic) stresses were introduced to account for all the residual stresses present in the deposited films. Later, a loading-unloading sequence was applied on the pre-stressed system, with a maximum normal load of 50N. The FEM also simulated the formation of the circular cracks by considering the presence of fifteen cracks distributed over the film surface and their propagation in the direction perpendicular to the film/substrate interface. Two different types of substrates and two different coatings were analyzed during the experiments. Substrates made of AA 6061 aluminum alloy and AISI 304 stainless steel were coated with (*i) titanium nitride (TiN) by unbalanced magnetron sputtering; and (*ii) silicon carbide (SiC) by plasma-enhanced chemical vapor deposition. Three thicknesses were studied in each of the four systems, which were later indented with normal loads of 50 N, applied by a sphere. The results indicated that, in each case, the array of circular cracks observed close to the contact edge usually develops with a similar inter-crack spacing, which has a strong relation with the film thickness and properties.
机译:在这项工作中,使用有限元方法(FEM)结合实验来研究在涂层系统压痕过程中观察到的一些裂纹模式。特别地,该研究集中在圆形裂纹阵列上,该圆形裂纹阵列靠近具有软质基材的系统的球形压痕的接触边缘。在FEM制定过程中考虑了一系列步骤。最初,引入沉积应力(本征)和热应力(本征)来解决存在于沉积膜中的所有残余应力。后来,在预应力系统上应用了加载-卸载序列,最大法向载荷为50N。有限元法还通过考虑在薄膜表面分布的十五个裂纹的存在及其在垂直于薄膜/基材界面的方向上的传播来模拟圆形裂纹的形成。在实验过程中分析了两种不同类型的基材和两种不同的涂层。由AA 6061铝合金和AISI 304不锈钢制成的基板通过不平衡磁控溅射镀有(* i)氮化钛(TiN); (* ii)通过等离子体增强化学气相沉积的碳化硅(SiC)。在这四个系统中的每个系统中研究了三个厚度,随后用球体施加了50 N的法向载荷压入。结果表明,在每种情况下,靠近接触边缘观察到的圆形裂纹阵列通常以相似的裂纹间距发展,这与膜的厚度和性能有很强的关系。

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