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Fabrication process of twin-free orthorhombic Nd123 single crystal under uni-axial compression

机译:单轴压缩下无孪晶正交Nd123单晶的制备工艺

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A fabrication process of twin-free orthorhombic NdBa_2Cu_3O_(7-#delta#) (Nd123) single crystals was studied, in which the as-grown tetragonal single crystals were directly annealed under uni-axial compression in order to fabricate the complete twin-free single crystals. Almost twinfree orthorhombic Nd123 single crystals could be obtained by modifying the annealing conditions from the viewpoint of the distribution of the oxygen contents and the release of the stress in the crystals during annealing. The critical current density (Jc)-H curves for the twin-free, the detwinned, and the not-detwinned Nd123 single crystals, which were affected by the Nd/Ba ratio fluctuation appearing in these crystals during annealing, showed a quite different tendency from those for YBa_2Cu_3O_(7-#delta) (Y123) single crystals.
机译:研究了无孪晶正交晶体的NdBa_2Cu_3O_(7-#delta#)(Nd123)单晶的制备工艺,其中,将生长的四方单晶直接在单轴压缩下进行退火,以制造完整的无孪晶。单晶。从退火过程中氧含量的分布和晶体中应力的释放的观点出发,通过改变退火条件,可以得到几乎无孪晶的斜方晶Nd123单晶。受退火过程中这些晶体中出现的Nd / Ba比波动影响的无孪晶,脱晶的和未脱晶的Nd123单晶的临界电流密度(Jc)-H曲线显示出完全不同的趋势由YBa_2Cu_3O_(7-delta)(Y123)单晶制成。

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