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MICRO-CT SCANNING STUDY ON EFFECT FACTORS OF SUBLIMATION INTERFACE DURING FREEZE-DRYING

机译:冻干过程中升华界面影响因素的微CT扫描研究

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Micro-CT scanner was used to follow the moving interface during sublimation. Apples slices used as experimental samples were scanned at certain time when drying. The scanning images were analyzed, then variation curves of grey value were obtained. To different thicknesses?¢freezing rates and primary drying temperatures, the different sublimation phenomena were compared. The results show that heat and mass exchange occurs both at the upper and the under surface of the sample. Also the exchange occurs at the side surface to some extent. To thick samples, the interface showing as a three-dimensional moving mode contracts to the geometric centre of the sample and presents approximate globosity. Samples frozen of slow freezing sublimate more quickly than those of quick freezing. The higher the primary drying temperature is, the more quickly sublimation interface moves. However, samples shrink and collapse more severely with high drying temperature under quick freezing condition.
机译:在升华过程中,使用Micro-CT扫描仪跟踪运动界面。干燥时,在一定时间扫描用作实验样品的苹果切片。对扫描图像进行分析,得到灰度值的变化曲线。针对不同的厚度,不同的冷冻速率和一次干燥温度,对不同的升华现象进行了比较。结果表明,热交换和质量交换都发生在样品的上表面和下表面。交换也在某种程度上在侧面发生。对于较厚的样品,显示为三维移动模式的界面会收缩到样品的几何中心,并呈现近似的球度。慢速冷冻的样品比速冻的样品升华更快。一次干燥温度越高,升华界面移动得越快。然而,在快速冷冻条件下,高干燥温度下样品会更严重地收缩和塌陷。

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