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A general procedure for evaluation of calibration baths in precision temperature measurements

机译:在精密温度测量中评估标定槽的通用程序

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The objective of the proposed paper is to develop a standardized procedure for evaluation of various calibration baths in precision temperature measurements. Since the uncertainties of transfer measurement and temperature standards such as SPRTs in particular are decreasing, metrological characteristics of calibration baths are becoming limiting factor in temperature calibrations by comparison. Due to the fact, that a time invariance of metrological characteristics of calibration baths (gradients, stability, repeatability, etc.) represents a major contribution to the total calibration uncertainty (providing known uncertainty of a standard thermometer), the exact knowledge about calibration bath is of an utmost importance. A general procedure for baths with different types of media (alcohol, water, silicon oil, fluidised alumina powder, etc.) is proposed, which enables continuous monitoring of bath parameters in order to properly evaluate uncertainty contributions to a measured (calibrated) thermometer. There is no ideal calibration system without inhomogeneity or gradient. Basic gradients that can be observed in calibration baths are axial and radial gradients. For the proper use of such a system in a process of calibration and measurement, gradients should be evaluated. Gradients appear as a change of the temperature reading of a thermometer due to a change of its position inside a calibration bath. A uniform profile and pre-defined points of calibration are under investigation. By this method a minimum uncertainty contribution could be defined as opposed to the maximum limit, thus enabling an optimal usage of particular calibration baths.
机译:拟议论文的目的是开发一种标准化程序,用于评估精密温度测量中的各种校准液。由于尤其是转移测量和温度标准(例如SPRT)的不确定性正在降低,因此,相比之下,校准槽的计量特性已成为温度校准的限制因素。由于以下事实,校准浴的计量特性(梯度,稳定性,可重复性等)的时间不变性代表了总校准不确定度(提供标准温度计的已知不确定度)的主要贡献,有关校准浴的确切知识至关重要。提出了一种使用不同介质(酒精,水,硅油,流化氧化铝粉等)的浴的通用程序,该程序可以连续监视浴参数,以便正确评估对测量(校准)温度计的不确定性影响。没有不均匀或没有梯度的理想校准系统。在校准液中可以观察到的基本梯度是轴向和径向梯度。为了在校准和测量过程中正确使用此类系统,应评估梯度。由于温度计在校准浴中的位置发生变化,因此梯度显示为温度计温度读数的变化。正在研究统一的轮廓和预定义的校准点。通过这种方法,可以定义与最大限制相反的最小不确定性贡献,从而可以最佳地使用特定的校准槽。

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