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Effects of a Large Content of Yttrium Doping on Microstructure and Magnetostriction of Fe_(83)Ga_(17) Alloy

机译:大量钇掺杂对Fe_(83)Ga_(17)合金的组织和磁致伸缩的影响

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As-cast (Fe_(0.83)Ga_(0.17))_(100-x)Y_x (x=0, 3, 6 and 9) alloys were prepared by non-consumable vacuum arc melting furnace under a protective argon atmosphere. The crystal structures and surface morphologies of the alloys were studied by X-ray diffraction (XRD), optical microscope (OM) and scanning electron microscopy (SEM), combined with energy dispersive spectroscopy (EDS), respectively. The surface domain structures were observed by atomic force microscopy (AFM). The magnetostriction coefficients of the alloys were measured by strain gauging method. The results showed that the as-cast Fe_(83)Ga_(17) alloy was composed only of a single phase of A2 with bcc structure, whereas the ternary Fe-Ga-Y alloys contain multiphase structure, besides the A2 phase, (FeGa)_(17)Y_(1.76) new phases are observed as well, and an elemental yttrium phase appeared when the yttrium content increased to x=6 and x=9. Doping with yttrium have an effect on the change of magnetic domain structure of the binary alloy. With increasing x, the magnetostriction coefficient of the (Fe_(0.83)Ga_(0.17))_(100-x)Y_x alloys decreased sharply. The minimum magnetostriction coefficient is reduced to 12 ppm at the magnetic field of 426kA/m when x=9.
机译:在保护性氩气气氛下,通过非消耗性真空电弧熔化炉制备铸态(Fe_(0.83)Ga_(0.17))_(100-x)Y_x(x = 0、3、6和9)合金。分别通过X射线衍射(XRD),光学显微镜(OM)和扫描电子显微镜(SEM)结合能量色散光谱(EDS)研究了合金的晶体结构和表面形态。通过原子力显微镜(AFM)观察表面域结构。通过应变测量法测量合金的磁致伸缩系数。结果表明,铸态Fe_(83)Ga_(17)合金仅由具有bcc结构的A2单相组成,而三元Fe-Ga-Y合金除A2相(FeGa )_(17)Y_(1.76)也观察到新相,并且当钇含量增加到x = 6和x = 9时出现元素钇相。钇掺杂对二元合金的磁畴结构变化有影响。随着x的增加,(Fe_(0.83)Ga_(0.17))_(100-x)Y_x合金的磁致伸缩系数急剧下降。当x = 9时,在426kA / m的磁场下,最小磁致伸缩系数降低到12 ppm。

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