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Low-stress coatings for sputtered-sliced Fresnel zone plates and multilayer Laue lenses

机译:溅射切片菲涅耳波带片和多层劳厄透镜的低应力涂层

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The application of thin film coating processes for the fabrication of diffractive X-ray optical elements like sputtered-sliced zone plates or multilayer Laue lenses (MLL) is a very promising approach for X-ray focusing down to spot sizes of < 10 nm. However, for practical useful focal length in the order of several millimeters or a few centimeters, multilayer thicknesses of several 10 μm up to a few 100 μm are necessary in order to have large enough numerical apertures of the lenses. Currently one of the main challenges is to coat low-stress multilayers with large total thicknesses in the order of 100 μm. Usually sputter deposition results in thin films with significant compressive stress. With new material combinations such as Mo/MoSi_2/Si/MoSi_2 and W/WSi_2/Si/WSi_2 the overall stress can be reduced to almost zero if the individual thicknesses are properly adapted. In the case of these four-layer-systems only the period thickness d_p follows the zone plate law. In case of Mo/MoSi_2/Si/MoSi_2, stress-free multilayers are obtained with d_(Mo) = 0.5~*d_p, d_(MoSi20 = 0.16~*d_p and d_(Si) = 0.34~*d_p.
机译:薄膜涂层工艺在制造衍射X射线光学元件(如溅射切片带状平板或多层Laue透镜(MLL))中的应用对于将X射线聚焦到小于10 nm的光斑非常有希望。然而,对于大约几毫米或几厘米的实用的有用焦距,为了具有足够大的透镜数值孔径,多层厚度必须在几十微米至几百微米之间。当前的主要挑战之一是涂覆低应力多层,其总厚度约为100μm。通常,溅射沉积导致薄膜具有明显的压缩应力。使用新的材料组合,例如Mo / MoSi_2 / Si / MoSi_2和W / WSi_2 / Si / WSi_2,如果适当地调整了各个厚度,则总应力可以降低到几乎为零。在这些四层系统中,只有周期厚度d_p遵循波带片定律。在Mo / MoSi_2 / Si / MoSi_2的情况下,获得的无应力多层具有d_(Mo)= 0.5〜* d_p,d_(MoSi20 = 0.16〜* d_p和d_(Si)= 0.34〜* d_p。

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