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Metal Injection Moulding of Nickel-Based Superalloy CM247LC

机译:镍基高温合金CM247LC的金属注射成型

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摘要

Metal Injection Moulding (MIM) is a promising new production technology for small to medium sizedparts with high geometric complexity as they are found in turbomachinery like aero engines orturbochargers. This study concerns the feasibility of manufacturing parts from nickel-based superalloyCM247LC via MIM and in particular the determination of optimum sintering and thermal processingparameters. CM247LC poses a serious challenge for MIM processing. Because of its high aluminumcontent, the strength potential is very high, but the sintering capability is severely restricted. Differentialscanning calorimetry (DSC) and dilatometry measurements as well as ThermoCalc simulations areused to optimize the sintering step of the MIM process route. Carbon, nitrogen and oxygen contents ofthe powder and the as sintered specimens are measured to evaluate the pick up of impurities duringprocessing. The microstructure of the as sintered specimens is characterized with respect to residualporosity, grain size and γ’ precipitation size and morphology. Room temperature strength andelongation in the MIM material are found to surpass conventional HIP material which is attributed tothe very fine grain size. Density and mechanical properties are observed to drop at the highestsintering temperatures. Ways to further improve the microstructure and strength will be discussed, inparticular for high temperature applications.
机译:金属注射成型(MIM)是一种有前途的新生产技术,适用于几何形状复杂的中小型零件,因为它们在航空机械(如航空发动机或涡轮增压器)中发现。这项研究涉及通过MIM由镍基超级合金CM247LC制造零件的可行性,尤其是确定最佳烧结和热处理参数的方法。 CM247LC对MIM处理提出了严峻的挑战。由于铝含量高,强度潜力很高,但烧结能力受到严重限制。差示扫描量热法(DSC)和膨胀计测量以及ThermoCalc模拟用于优化MIM工艺路线的烧结步骤。测量粉末和烧结样品的碳,氮和氧含量,以评估加工过程中杂质的吸收。烧结后的试样的微观结构在残余孔隙率,晶粒尺寸以及γ'沉淀尺寸和形貌方面得到了表征。发现MIM材料中的室温强度和伸长率超过常规的HIP材料,这归因于非常细的晶粒尺寸。在最高的烧结温度下观察到密度和机械性能下降。将讨论进一步改善微观结构和强度的方法,尤其是在高温应用中。

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    Joint Institute of Advanced Materials and Processes (ZMP) Friedrich-Alexander-Universität Erlangen-Nürnberg Dr.-Mack-Straße 81 90762 Fürth Germany andreas.j.meyer@fau.de;

    Rolls-Royce Deutschland Ltd Co KG Eschenweg 11 Dahlewitz 15827 Blankenfelde-Mahlow Germany Enrico.Daenicke@rolls-royce.com;

    Rolls-Royce Deutschland Ltd Co KG Eschenweg 11 Dahlewitz 15827 Blankenfelde-Mahlow Germany Katharina.Horke@Rolls-Royce.com;

    Rolls-Royce Deutschland Ltd Co KG Eschenweg 11 Dahlewitz 15827 Blankenfelde-Mahlow Germany;

    Schunk Sintermetalltechnik GmbH Rosstrappenstraße 62 06502 Thale Germany sieglinde.mueller@schunk-group.com;

    Schunk Sintermetalltechnik GmbH Rosstrappenstraße 62 06502 Thale Germany ingolf.langer@schunk-group.com;

    Joint Institute of Advanced Materials and Processes (ZMP) Friedrich-Alexander-Universität Erlangen-Nürnberg Dr.-Mack-Straße 81 90762 Fürth Germany robert.singer@ww.uni-erlangen.de;

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