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Synthesis, characterization and photocatalytic activity of Co2+-doped titania

机译:Co2 +掺杂二氧化钛的合成,表征及光催化活性

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Photocatalyst of Co2+-doped titania was simply prepared, and the photocatalytic activity was tested under UV irradiation for methyl orange degradation. The influence of doping quantity, calcination temperature, calcination time and quantity of catalyst was investigated for photocatalytic efficiency of the photocatalyst. The sample was characterized by UV diffuse reflectance spectra (UV/DRS), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) and IR. The results showed that the photocatalytic activity Co2+-doped TiO2 which calcined at 200 ℃for 5 h is high, and which diameter is about 4-7 run presents anatase phase. The sample absorption band of UV/DRS moves to visible region and reaches 580 nm. This kind of catalyst is also effective for degradation other organic dyes and beer wastewater.
机译:简单地制备了掺杂Co 2+的二氧化钛的光催化剂,并在紫外线照射下测试了甲基橙降解的光催化活性。研究了掺杂量,煅烧温度,煅烧时间和催化剂用量对光催化剂光催化效率的影响。样品通过紫外漫反射光谱(UV / DRS),X射线衍射(XRD),X射线光电子能谱(XPS),透射电子显微镜(TEM)和IR进行表征。结果表明,在200℃煅烧5 h的Co2 +掺杂的TiO2具有较高的光催化活性,其直径约为4-7nm呈锐钛矿相。 UV / DRS的样品吸收带移至可见光区域并达到580 nm。这种催化剂对降解其他有机染料和啤酒废水也有效。

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