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Synthesis of nanosize aluminum powders by electrical explosion of wire in the gaseous media

机译:气体介质中金属丝的电爆炸合成纳米铝粉

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The wire electrical explosion (WEE) method is a new gas-phase synthesis method for the production of nanosize powders. And the WEE method has the advantages of high energy efficiency and high purity through the production under pure inert gas conditions. In the paper, an experimental device based on the electrical explosion of metallic wires for the nanopowders production and collection was designed and built. Also, aluminum nanopowders were produced by electrical exploding aluminum wire and collected by the microporous membrane filter successfully under different experimental conditions. And the influence of these experimental conditions on the characteristics of aluminum nanopowders was analyzed by the transmission electron microscope images. Moreover, the discharge channel structure upon electrical explosion of wires was studied by the high-speed framing camera. The results showed that the size and composition of the aluminum nanoparticles can be controlled by many parameters, such as the energy-storage capacitor and its charging voltage, the gaseous media as well as their pressures and temperature, the wire materials and its diameters. However, only the influences of the electrical energy entering the wire and the pressure of surrounding gas on the dimension of the aluminum nanopowders were discussed in detail.
机译:线电爆炸(WEE)方法是一种用于生产纳米级粉末的新型气相合成方法。通过在纯惰性气体条件下生产,WEE方法具有高能效和高纯度的优点。本文设计并建立了一种基于金属丝电爆炸的实验装置,用于纳米粉的生产和收集。此外,通过电爆炸铝丝生产铝纳米粉,并在不同的实验条件下成功地通过微孔膜过滤器将其收集。并通过透射电镜图像分析了这些实验条件对铝纳米粉体性能的影响。此外,通过高速成帧照相机研究了电线电爆炸时的放电通道结构。结果表明,铝纳米颗粒的尺寸和组成可以通过许多参数控制,例如储能电容器及其充电电压,气态介质及其压力和温度,线材及其直径。然而,仅详细讨论了进入金属丝的电能和周围气体的压力对铝纳米粉体尺寸的影响。

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