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Ultrananocrystalline diamond tip integrated onto a heated atomic force microscope cantilever

机译:超纳米晶金刚石尖端集成到加热的原子力显微镜悬臂上

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We report a wear-resistant ultrananocrystalline (UNCD) diamond tip integrated onto a heated atomic force microscope (AFM) cantilever and UNCD tips integrated into arrays of heated AFM cantilevers. The UNCD tips are batch-fabricated and have apex radii of approximately 10 nm and heights up to 7 μm. The solid-state heater can reach temperatures above 600 °C and is also a resistive temperature sensor. The tips were shown to be wear resistant throughout 1.2 m of scanning on a single-crystal silicon grating at a force of 200 nN and a speed of 10 μm s~(-1). Under the same conditions, a silicon tip was completely blunted. We demonstrate the use of these heated cantilevers for thermal imaging in both contact mode and intermittent contact mode, with a vertical imaging resolution of 1.9 nm. The potential application to nanolithography was also demonstrated, as the tip wrote hundreds of polyethylene nanostructures.
机译:我们报告了将耐磨的超纳米晶(UNCD)金刚石尖端集成到加热的原子力显微镜(AFM)悬臂上,并将UNCD尖端集成到加热的AFM悬臂阵列中。 UNCD尖端是分批制造的,其顶点半径约为10 nm,高度可达7μm。固态加热器可以达到600°C以上的温度,并且还是电阻温度传感器。结果表明,在200 nN的力和10μms〜(-1)的速度下,在单晶硅光栅上扫描1.2 m时,尖端具有耐磨性。在相同条件下,硅尖端完全钝化。我们演示了使用这些加热的悬臂在接触模式和间歇接触模式下进行热成像,垂直成像分辨率为1.9 nm。当笔尖写了数百个聚乙烯纳米结构时,还展示了在纳米光刻技术上的潜在应用。

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