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Fabrication and buckling dynamics of nanoneedle AFM probes

机译:纳米针原子力显微镜探针的制备和屈曲动力学

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摘要

A new method for the fabrication of high-aspect-ratio probes by electron beam induced deposition is described. This technique allows the fabrication of cylindrical 'nanoneedle' structures on the atomic force microscope (AFM) probe tip which can be used for accurate imaging of surfaces with high steep features. Scanning electron microscope (SEM) imaging showed that needles with diameters in the range of 18-100nm could be obtained by this technique. The needles were shown to undergo buckling deformation under large tip-sample forces. The deformation was observed to recover elastically under vertical deformations of up to ~ 60% of the needle length, preventing damage to the needle. A technique of stabilizing the needle against buckling by coating it with additional electron beam deposited carbon was also investigated; it was shown that coated needles of 75nm or greater total diameter did not buckle even under tip-sample forces of ~ 1.5νN.
机译:描述了一种通过电子束诱导沉积制造高纵横比探针的新方法。该技术允许在原子力显微镜(AFM)探针头上制造圆柱形的“纳米酮”结构,该结构可用于对具有高陡度特征的表面进行精确成像。扫描电子显微镜(SEM)成像表明,通过该技术可以得到直径在18-100nm范围内的针。针头在较大的针头采样力作用下会发生屈曲变形。观察到该变形在高达针长的约60%的垂直变形下可弹性恢复,从而防止损坏针。还研究了通过用额外的电子束沉积碳涂覆针头来稳定针头以防止屈曲的技术。结果表明,即使在〜1.5νN的针尖采样力下,总直径为75nm或更大的涂层针也不会弯曲。

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