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Structural and magnetic characterization of Pd nanoparticles encapsulated in apoferritin

机译:去铁铁蛋白包封的Pd纳米颗粒的结构和磁性表征

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摘要

Pd nanoparticles exhibiting permanent magnetism at room temperature have been prepared within the apoferritin cavity. Pd nanoparticles in air and under an inert atmosphere were synthesized to study the influence of the aerobic and anaerobic conditions in the final magnetic properties. The surface of nanoparticles as well as the type of crystalline phase could determine the magnetic properties. X-ray powder diffraction, including Debye-function analysis, transmission electronic microscopy, and magnetization measurements have been used for characterizing the nanoparticles.
机译:已经在脱铁铁蛋白腔内制备了在室温下表现出永久磁性的Pd纳米颗粒。合成了空气中和惰性气氛下的Pd纳米粒子,以研究好氧和厌氧条件对最终磁性的影响。纳米粒子的表面以及晶相的类型可以决定磁性。 X射线粉末衍射(包括德拜功能分析,透射电子显微镜和磁化测量)已用于表征纳米粒子。

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