Synthesis and characterization of silver(I) complexes [AgL]_2[BF_4]_2 and [Ag(OAc)L]_infinity [L=(CH_2NHCOC_2H_4PPh_2)_2]

Yat Li; Ka-Fu Yung; Hoi-Shan Chan; Wing-Tak Wong; Wai-Kwok Wong; Man-Chung Tse

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Synthesis and characterization of silver(I) complexes [AgL]_2[BF_4]_2 and [Ag(OAc)L]_infinity [L=(CH_2NHCOC_2H_4PPh_2)_2]

机译：银（I）配合物[AgL] _2 [BF_4] _2和[Ag（OAc）L] _infinity [L =（CH_2NHCOC_2H_4PPh_2）_2]的合成与表征

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The interaction of (CH_2NHCOC_2H_4PPh_2)_2,L,with one equivalent of AgBF_4 and AgOAc gave [AgL]_2[BF_4]_2 1 and [Ag(OAc)L]_infinity 2,respectively.X-ray crystallographic studies showed that the ligand adopts a linear conformation in dimeric complex 1 and a bent conformation in polymeric complex 2.Both compounds exhibited temperature-dependent ~31P{1H} NMR spectra.

机译：（CH_2NHCOC_2H_4PPh_2）_2，L与一当量的AgBF_4和AgOAc的相互作用分别产生[AgL] _2 [BF_4] _2 1和[Ag（OAc）L] _infinity2。X射线晶体学研究表明该配体采用二聚体1中的线性构象和聚合体2中的弯曲构象。这两种化合物均表现出温度依赖性〜31P {1H} NMR光谱。

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来源
《Inorganic Chemistry Communications》 |2003年第10期|共4页
作者
Yat Li; Ka-Fu Yung; Hoi-Shan Chan; Wing-Tak Wong; Wai-Kwok Wong; Man-Chung Tse;
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正文语种 eng
中图分类无机化学;
关键词
silver(I) complex; Bis(ethylamidophosphine); crystal structure; temperature-dependent ~31P{~1H} NMR study;

机译：银（I）配合物;双（乙基氨基膦）;晶体结构;温度依赖性〜31P {〜1H} NMR研究;

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1. Synthesis and characterization of silver(I) complexes [AgL]_2[BF_4]_2 and [Ag(OAc)L]_infinity [L=(CH_2NHCOC_2H_4PPh_2)_2] [J] . Yat Li, Ka-Fu Yung, Hoi-Shan Chan, Inorganic Chemistry Communications . 2003,第10期

机译：银（I）配合物[AgL] _2 [BF_4] _2和[Ag（OAc）L] _infinity [L =（CH_2NHCOC_2H_4PPh_2）_2]的合成与表征
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Synthesis and characterization of silver(I) complexes [AgL]_2[BF_4]_2 and [Ag(OAc)L]_infinity [L=(CH_2NHCOC_2H_4PPh_2)_2]

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