[SnI8{Fe(CO)4}4]2+ Highly Coordinated Sn+III8 Subunit with Fragile Carbonyl Clips

摘要

Abstract > [SnI <sub>8</sub> {Fe(CO) <sub>4</sub> } <sub>4</sub> ][Al <sub>2</sub> Cl <sub>7</sub> ] <sub>2</sub> contains the [SnI <sub>8</sub> {Fe(CO) <sub>4</sub> } <sub>4</sub> ] 2+ cation with an unprecedented highly coordinated, bicapped SnI <sub>8</sub> prism. Given the eightfold coordination with the most voluminous stable halide, it is all the more surprising that this SnI <sub>8</sub> arrangement is surrounded only by fragile Fe(CO) <sub>4</sub> groups in a clip‐like fashion. Inspite of a predominantly ionic bonding situation in [SnI <sub>8</sub> {Fe(CO) <sub>4</sub> } <sub>4</sub> ] 2+ , the I ? ???I ? distances are considerably shortened (down to 371?pm) and significantly less than the van der Waals distance (420?pm). The title compound is characterized by single‐crystal structure analysis, spectroscopic methods (EDXS, FTIR, Raman, UV/Vis, M?ssbauer), thermogravimetry, and density functional theory methods. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > [Sni. <sub> 8 </ sub> {Fe（CO） <sub> 4 </ sub> } <sub> 4 </ sub> ] [al. <sub> 2 </ sub> CL. <sub> 7 </ sub> ] <sub> 2 </ sub> 包含[SNI <sub> 8 </ sub> {Fe（CO） <sub> 4 </ sub> } <sub> 4 </ sub> ] 2 + </ sup> 与前所未有的高度协调，双重的Sni <sub> 8 </ sub> 棱镜。鉴于与最大稳定的卤化物的八倍协调，这令人惊讶的是这个SNI <sub> 8 </ sub> 安排仅被脆弱的Fe（CO）包围 <sub> 4 </ sub> 以剪辑的方式群体。在[SNI中主要的离子粘合情况 <sub> 8 </ sub> {Fe（CO） <sub> 4 </ sub> } <sub> 4 </ sub> ] 2 + </ sup> ，我？</ sup> ？？？一世？</ sup> 距离显着缩短（低至371℃），明显小于范德瓦尔斯距离（420？PM）。标题化合物的特征在于单晶结构分析，光谱法（EDXS，FTIR，拉曼，UV / Vis，M 2 Ssbauer），热重率和密度泛函理论方法。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第14期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=carbonyl ligands&option=203" rel="nofollow">carbonyl ligands;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ionic liquids&option=203" rel="nofollow">ionic liquids;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=SnI8&option=203" rel="nofollow">SnI8;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tin iodide&option=203" rel="nofollow">tin iodide;</a> </p> <div class="translation"> 机译：羰基配体;离子液体;SNI8;锡碘化物; 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