Atomic‐Scale Mapping of Impurities in Partially Reduced Hollow TiO2 Nanowires

摘要

Abstract > The incorporation of impurities during the chemical synthesis of nanomaterials is usually uncontrolled and rarely reported because of the formidable challenge in measuring trace amounts of often light elements with sub‐nanometer spatial resolution. And yet, these foreign elements (introduced by doping, for example) influence functional properties. We demonstrate how the hydrothermal growth and a partial reduction reaction on hollow TiO <sub>2</sub> nanowires leads to the introduction of parts per millions of boron, sodium, and nitrogen. This doping explains the presence of oxygen vacancies and reduced Ti states at the surface, which enhance the functional properties of TiO <sub>2</sub> . Our results were obtained on model metal oxide nanomaterials and they shed light on a general process that leads to the uncontrolled incorporation of trace impurities in TiO <sub>2</sub> , thereby, having a strong effect on applications in energy‐harvesting. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 在纳米材料的化学合成期间掺入杂质通常是不受控制的并且很少报道，因为在测量具有亚纳米空间分辨率的痕量的通常光元件中的痕量痕量时，很少报道。然而，这些异物（例如通过掺杂引入）影响功能性质。我们展示了水热生长和空心TiO上的部分还原反应 <sub> 2 </ sub> 纳米线导致每百万硼，钠和氮气引入零件。该掺杂解释了氧空位的存在并在表面上减少了Ti状态，增强了TiO的功能性质 <sub> 2 </ sub> 。我们的结果是在模型金属氧化物纳米材料上获得的，并且它们在一般过程中脱光，导致TiO中的痕量杂质的不受控制的掺入 <sub> 2 </ sub> 由此，对能量收集中的应用具有强烈影响。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第14期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=atom probe tomography&option=203" rel="nofollow">atom probe tomography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electron microscopy&option=203" rel="nofollow">electron microscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=impurities&option=203" rel="nofollow">impurities;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=oxygen vacancies&option=203" rel="nofollow">oxygen vacancies;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=TiO2&option=203" rel="nofollow">TiO2;</a> </p> <div class="translation"> 机译：原子探测断层扫描;电子显微镜;杂质;氧气空位;TiO2; 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href="/conference-cn-6185/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第七届全国环境化学学术大会 </a> <span> <span> . 2013</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314945384.html">纳米TiO2、SnO2/TiO2(空心)复合光催化剂的制备、表征及光催化性能研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=吴飞妹&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 吴飞妹</a> <span> . 2014</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061202569682.html">SiO2‑介孔TiO2空心微球封装纳米金环己烷氧化催化剂及其制备和应用</a> <b>[P]</b> . <span> 中国专利： CN105327717B </span> <span> . 2017.09.15</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120107829214.html">SiO2-介孔TiO2空心微球封装纳米金环己烷氧化催化剂及其制备和应用</a> <b>[P]</b> . <span> 中国专利： CN105327717A </span> <span> . 2016-02-17</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130421882223.html">manufacturing method for hybrid photoelectrode consisting of vertically aligned TiO2 nanowire and mesoporous TiO2 films infiltrated between TiO2 nanowires</a> <b>[P]</b> . <span> 外国专利：  KR101198325B1 </span> <span> . 2012-11-06</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：垂直排列的TiO2纳米线和渗透在TiO2纳米线之间的介孔TiO2膜组成的混合光电极的制备方法 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130421882236.html">manufacturing method for hybrid photoelectrode consisting of vertically aligned TiO2 nanowire and TiO2 nanoparticles fabricated by 2-step hydrothermal process</a> <b>[P]</b> . <span> 外国专利：  KR101198310B1 </span> <span> . 2012-11-07</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：两步水热法制备由垂直取向的TiO2纳米线和TiO2纳米粒子组成的混合光电极的制备方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130487412315.html">A method for removing rust, scale, rolling skin and kieselsaeurehaltigen detected or impurities from the inner surface of hollow bodies and hollow body systems, such as, for example, boiler plants and pipelines, by means of a dressing as a function of the flue sig</a> <b>[P]</b> . <span> 外国专利：  DE1621596A1 </span> <span> . 1971-06-03</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：一种根据烟道信号通过敷料去除中空物体和中空物体系统（例如锅炉设备和管道）内表面的锈蚀，水垢，滚动的皮肤和硅藻土氨氮或杂质的方法 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> 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