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首页> 外文期刊>Angewandte Chemie >High‐Resolution Electrochemical Mapping of the Hydrogen Evolution Reaction on Transition‐Metal Dichalcogenide Nanosheets
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High‐Resolution Electrochemical Mapping of the Hydrogen Evolution Reaction on Transition‐Metal Dichalcogenide Nanosheets

机译：氢进化反应对转型金属二甲基甲基纳米液的高分辨率电化学映射

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摘要

Abstract > High‐resolution scanning electrochemical cell microscopy (SECCM) is used to image and quantitatively analyze the hydrogen evolution reaction (HER) catalytically active sites of 1H‐MoS <sub>2</sub> nanosheets, MoS <sub>2</sub> , and WS <sub>2</sub> heteronanosheets. Using a 20?nm radius nanopipette and hopping mode scanning, the resolution of SECCM was beyond the optical microscopy limit and visualized a small triangular MoS <sub>2</sub> nanosheet with a side length of ca. 130?nm. The electrochemical cell provides local cyclic voltammograms with a nanoscale spatial resolution for visualizing HER active sites as electrochemical images. The HER activity difference of edge, terrace, and heterojunction of MoS <sub>2</sub> and WS <sub>2</sub> were revealed. The SECCM imaging directly visualized the relationship of HER activity and number of MoS <sub>2</sub> nanosheet layers and unveiled the heterogeneous aging state of MoS <sub>2</sub> nanosheets. SECCM can be used for improving local HER activities by producing sulfur vacancies using electrochemical reaction at the selected region. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 高分辨率扫描电化学电池显微镜（SECCM）用于图像和定量分析1H-MOS的催化活性位点的氢进化反应（她） <sub> 2 </ sub> Nanosheets，Mos. <sub> 2 </ sub> 和ws. <sub> 2 </ sub> horidOnanosheets。使用20？NM半径纳米纤维和跳跃模式扫描，Seccm的分辨率超出了光学显微镜限制，可视化了一个小三角形MOS <sub> 2 </ sub> 纳米片具有侧面长度的CA。 130？nm。电化学电池提供局部循环伏安图，其具有纳米级空间分辨率，用于可视化其活性位点作为电化学图像。她的边缘，露台和MOS的异性结的活动差异 <sub> 2 </ sub> 和ws. <sub> 2 </ sub> 被揭露了。 SECCM成像直接可视化她的活动和MOS数量的关系 <sub> 2 </ sub> 纳米片层并揭开了MOS的异质老化状态 <sub> 2 </ sub> nanosheets。 Seccm可用于通过在所选区域的电化学反应产生硫空位来改善局部活动。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第9期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Takahashi Yasufumi&option=202" target="_blank" rel="nofollow">Takahashi Yasufumi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kobayashi Yu&option=202" target="_blank" rel="nofollow">Kobayashi Yu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Wang Ziqian&option=202" target="_blank" rel="nofollow">Wang Ziqian;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ito Yoshikazu&option=202" target="_blank" rel="nofollow">Ito Yoshikazu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ota Masato&option=202" target="_blank" rel="nofollow">Ota Masato;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Ida Hiroki&option=202" target="_blank" rel="nofollow">Ida Hiroki;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kumatani Akichika&option=202" target="_blank" rel="nofollow">Kumatani Akichika;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miyazawa Keisuke&option=202" target="_blank" rel="nofollow">Miyazawa Keisuke;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fujita Takeshi&option=202" target="_blank" rel="nofollow">Fujita Takeshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Shiku Hitoshi&option=202" target="_blank" rel="nofollow">Shiku Hitoshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Korchev Yuri E.&option=202" target="_blank" rel="nofollow">Korchev Yuri E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Miyata Yasumitsu&option=202" target="_blank" rel="nofollow">Miyata Yasumitsu;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Fukuma Takeshi&option=202" target="_blank" rel="nofollow">Fukuma Takeshi;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Chen Mingwei&option=202" target="_blank" rel="nofollow">Chen Mingwei;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Matsue Tomokazu&option=202" target="_blank" rel="nofollow">Matsue Tomokazu;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>WPI Nano Life Science Institute (NanoLSI WPI)Kanazawa University Kakuma-machiKanazawa Ishikawa 920-1192 Japan;</p> <p>Department of PhysicsTokyo Metropolitan University HachiojiTokyo 192-0397 Japan;</p> <p>Department of Materials Science and EngineeringJohns Hopkins UniversityBaltimore MD 21218 USA;</p> <p>Precursory Research for Embryonic Science and Technology (PRESTO) (Japan)Science and Technology Agency (JST)Saitama 332-0012 Japan;</p> <p>WPI Nano Life Science Institute (NanoLSI WPI)Kanazawa University Kakuma-machiKanazawa Ishikawa 920-1192 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11-604 Aramaki Aoba Aoba-ku Sendai 980-8579 Japan;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11-604 Aramaki Aoba Aoba-ku Sendai 980-8579 Japan;</p> <p>WPI Nano Life Science Institute (NanoLSI WPI)Kanazawa University Kakuma-machiKanazawa Ishikawa 920-1192 Japan;</p> <p>School of Environmental Science and EngineeringKochi University of TechnologyKochi 782-8502 Japan;</p> <p>Department of Applied ChemistryTohoku UniversitySendai 980-8579 Japan;</p> <p>WPI Nano Life Science Institute (NanoLSI WPI)Kanazawa University Kakuma-machiKanazawa Ishikawa 920-1192 Japan;</p> <p>Department of PhysicsTokyo Metropolitan University HachiojiTokyo 192-0397 Japan;</p> <p>WPI Nano Life Science Institute (NanoLSI WPI)Kanazawa University Kakuma-machiKanazawa Ishikawa 920-1192 Japan;</p> <p>Department of Materials Science and EngineeringJohns Hopkins UniversityBaltimore MD 21218 USA;</p> <p>Graduate School of Environmental StudiesTohoku University6-6-11-604 Aramaki Aoba Aoba-ku Sendai 980-8579 Japan;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electrochemistry&option=203" rel="nofollow">electrochemistry;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrogen evolution reaction&option=203" rel="nofollow">hydrogen evolution reaction;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=MoS2&option=203" rel="nofollow">MoS2;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=scanning electrochemical cell microscopy&option=203" rel="nofollow">scanning electrochemical cell microscopy;</a> </p> <div class="translation"> 机译：电化学;氢气进化反应;MOS2;扫描电化学细胞显微镜; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div 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href="/patent-detail/06120104464930.html">由其它二甲基萘异构体和由各环上具有一个甲基的二甲基四氢萘/二甲基十氢萘制备2,6－二甲基萘的方法</a> <b>[P]</b> . <span> 中国专利： CN1263518A </span> <span> . 2000-08-16</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130400752897.html">COMPLEX COMPRISING TRANSITION METAL DICHALCOGENIDE NANOPARTICLE AND TRANSITION METAL DICHALCOGENIDE NANOSHEET, METHOD FOR MANUFACTURING SAME, AND CATALYST FOR HYDROGEN EVOLUTION REACTION COMPRISING SAME</a> <b>[P]</b> . <span> 外国专利： <!-- 韩国专利： --> KR20200039192A </span> <span> . 2020-04-16</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包含过渡金属二氢萘类纳米粒子和过渡金属二氢萘类纳米粒子的复合物，其制备方法以及包含相同氢原子发生反应的催化剂 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130500184066.html">GRAPHENE-TRANSITION METAL CATALYST FOR HYDROGEN EVOLUTION REACTION</a> <b>[P]</b> . <span> 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