A Directed Route to Colloidal Nanoparticle Synthesis of the Copper Selenophosphate Cu3PSe4

Lee Jennifer M.; Kraynak Leslie A.; Prieto Amy L.

摘要

Abstract > The first colloidal nanoparticle synthesis of the copper selenophosphate Cu <sub>3</sub> PSe <sub>4</sub> , a promising new material for photovoltaics, is reported. Because the formation of binary copper selenide impurities seemed to form more readily, two approaches were developed to install phosphorus bonds directly: 1)?the synthesis of molecular P <sub>4</sub> Se <sub>3</sub> and subsequent reaction with a copper precursor, (P‐Se)+Cu, and 2)?the synthesis of copper phosphide, Cu <sub>3</sub> P, nanoparticles and subsequent reaction with a selenium precursor, (Cu‐P)+Se. The isolation and purification of Cu <sub>3</sub> P nanoparticles and subsequent selenization yielded phase‐pure Cu <sub>3</sub> PSe <sub>4</sub> . Solvent effects and Se precursor reactivities were elucidated and were key to understanding the final reaction conditions. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 第一胶体纳米粒子合成硒磷酸铜Cu <sub> 3 </ sub> PSE. <sub> 4 </ sub> 据报道，光伏光伏的新材料。因为二元铜硒化杂物杂质的形成似乎更容易形成，所以开发了两种方法以直接安装磷键：1）？分子p的合成 <sub> 4 </ sub> se <sub> 3 </ sub> 并随后与铜前体的反应（p-SE）+ Cu和2）？合成磷化铜，Cu <sub> 3 </ sub> P，纳米颗粒和随后与硒前体的反应（Cu-P）+ Se。 Cu的分离和纯化 <sub> 3 </ sub> P纳米粒子和随后的硒化产生相纯Cu <sub> 3 </ sub> PSE. <sub> 4 </ sub> 。阐明了溶剂效应和SE前体反应性，并是理解最终反应条件的关键。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第8期</span><b style="margin: 0 2px;">|</b><span>共5页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Lee Jennifer M.&option=202" target="_blank" rel="nofollow">Lee Jennifer M.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kraynak Leslie A.&option=202" target="_blank" rel="nofollow">Kraynak Leslie A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Prieto Amy L.&option=202" target="_blank" rel="nofollow">Prieto Amy L.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryColorado State UniversityFort Collins CO 80523 USA;</p> <p>Department of ChemistryColorado State UniversityFort Collins CO 80523 USA;</p> <p>Department of ChemistryColorado State UniversityFort Collins CO 80523 USA;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=colloidal nanoparticles&option=203" rel="nofollow">colloidal nanoparticles;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=copper selenophosphate&option=203" rel="nofollow">copper selenophosphate;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hard–soft acid–base principle&option=203" rel="nofollow">hard–soft acid–base principle;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=reaction pathways&option=203" rel="nofollow">reaction pathways;</a> </p> <div class="translation"> 机译：胶体纳米颗粒;硒磷酸铜;硬酸碱基础原则;反应途径; 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陆娟</a> <span> . 2020</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120108535876.html">铜纳米粒子及其制造方法、铜纳米粒子分散液、铜纳米油墨、铜纳米粒子的保存方法和铜纳米粒子的烧结方法</a> <b>[P]</b> . <span> 中国专利： CN106029261A </span> <span> . 2016-10-12</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120111180501.html">一步合成团簇型钯铜纳米粒子的方法及团簇型钯铜纳米粒子的应用</a> <b>[P]</b> . <span> 中国专利： CN108672717A </span> <span> . 2018-10-19</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130403982680.html">The process of the application of coconut water as a reducing agent in the route of synthesis of nanoparticles of gold, silver, copper and iron.</a> <b>[P]</b> . <span> 外国专利：  BR102017011632A2 </span> <span> . 2018-12-18</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：在金，银，铜和铁的纳米颗粒的合成路线中应用椰子水作为还原剂的过程。 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130403284387.html">SYNTHESIS OF COPPER NANOPARTICLES MANUFACTURED BY USING CARBIDE-BASED ELECTRIDE AND ORGANIC COPPER COMPOUNDS AND MANUFACTURING OF CONDUCTIVE INK BY USING COPPER NANOPARTICLES</a> <b>[P]</b> . <span> 外国专利：  KR20190055678A </span> <span> . 2019-05-23</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：硬质合金和有机铜化合物制备铜纳米粒子的合成及铜纳米粒子制备导电油墨 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130400742988.html">MANUFACTURING METHOD OF COPPER-TITANIUM NANOPARTICLES BY HYDROTHERMAL SYNTHESIS METHOD, COPPER-TITANIUM NANOPARTICLES BY SAME AND ANTIBACTERIAL LATEX FOAM CONTAINING SAME</a> <b>[P]</b> . <span> 外国专利：  KR20200049005A </span> <span> . 2020-05-08</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：水热合成法制备铜钛纳米粒子，相同方法制备铜钛纳米粒子和同时含有抗菌乳胶的泡沫钛合金纳米粒子 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704028161900','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> <p 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