Single‐Crystal X‐Ray Diffraction Study of Pressure and Temperature‐Induced Spin Trapping in a Bistable Iron(II) Hofmann Framework

Turner Gemma F.; Campbell Fallyn; Moggach Stephen A.; Parsons Simon; Goeta Andrés E.; Mu?oz M. Carmen; Real José A.

摘要

Abstract > High‐pressure single‐crystal X‐ray diffraction has been used to trap both the low‐spin (LS) and high‐spin (HS) states of the iron(II) Hofmann spin crossover framework, [Fe II (pdm)(H <sub>2</sub> O)[Ag(CN) <sub>2</sub> ] <sub>2</sub> ?H <sub>2</sub> O, under identical experimental conditions, allowing the structural changes arising from the spin‐transition to be deconvoluted from previously reported thermal effects. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 高压单晶X射线衍射已被用于捕获铁（II）霍夫曼旋转交叉框架的低旋转（LS）和高旋转（HS）状态，[FE ii </ sup> （pdm）（h <sub> 2 </ sub> o）[ag（cn） <sub> 2 </ sub> ] <sub> 2 </ sub> ？H <sub> 2 </ sub> o在相同的实验条件下，允许从旋转过渡产生的结构变化从先前报告的热效应中被解作消除。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第8期</span><b style="margin: 0 2px;">|</b><span>共6页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Turner Gemma F.&option=202" target="_blank" rel="nofollow">Turner Gemma F.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Campbell Fallyn&option=202" target="_blank" rel="nofollow">Campbell Fallyn;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Moggach Stephen A.&option=202" target="_blank" rel="nofollow">Moggach Stephen A.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Parsons Simon&option=202" target="_blank" rel="nofollow">Parsons Simon;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Goeta Andrés E.&option=202" target="_blank" rel="nofollow">Goeta Andrés E.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mu?oz M. Carmen&option=202" target="_blank" rel="nofollow">Mu?oz M. Carmen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Real José A.&option=202" target="_blank" rel="nofollow">Real José A.;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of Molecular Sciences/Centre for Microscopy Characterisation and AnalysisThe University of Western Australia35 Stirling Highway Crawley Perth WA 6009 Australia;</p> <p>EastChem School of Chemistry and Centre for Science at Extreme ConditionsThe University of EdinburghKings Buildings West Mains Road Edinburgh EH9 3JJ UK;</p> <p>School of Molecular Sciences/Centre for Microscopy Characterisation and AnalysisThe University of Western Australia35 Stirling Highway Crawley Perth WA 6009 Australia;</p> <p>EastChem School of Chemistry and Centre for Science at Extreme ConditionsThe University of EdinburghKings Buildings West Mains Road Edinburgh EH9 3JJ UK;</p> <p>Department of ChemistryDurham UniversitySouth Road Durham DH1 3LE UK;</p> <p>Departamento de Física AplicadaUniversitat Politècnica de ValènciaCamino de Vera s/n 46022 Valéncia Spain;</p> <p>Institut de Ciencia Molecular/ Departament de Quimica InorganicaUniversitat de ValènciaDoctor Moliner 50 46100 Burjassot València Spain;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=iron complexes&option=203" rel="nofollow">iron complexes;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=high-pressure crystallography&option=203" rel="nofollow">high-pressure crystallography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hofmann framework&option=203" rel="nofollow">Hofmann framework;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=spin-crossover&option=203" rel="nofollow">spin-crossover;</a> </p> <div class="translation"> 机译：铁复合物;高压晶体学;Hofmann框架;旋转交叉; 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<span> <a href="/journal-cn-5605/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国农村卫生 </a> </span> <span> . 2018</span><span>,第002期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-32964_thesis/02022717587.html">尺度旋转在图像恢复中的运用研究</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陆俊&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陆俊</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=迟男&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,迟男</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=阮秋琦&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,阮秋琦</a> <span> <a href="/conference-cn-32964/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 中国电子学会第五届青年学术年会 </a> <span> <span> . 1999</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314568487.html">温度对单晶硅表面摩擦诱导选择性刻蚀的影响研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=金晨宁&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 金晨宁</a> <span> . 2017</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120100123881.html">一种铁（III）四羧基苯基卟啉植入金属有机框架的制备和应用</a> <b>[P]</b> . <span> 中国专利： CN109126877A </span> <span> . 2019-01-04</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120104074828.html">一种分子荧光探针晶态材料及其在铬（VI）和铁（III）离子检测中的应用</a> <b>[P]</b> . <span> 中国专利： CN111484511A </span> <span> . 2020-08-04</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130490187230.html">X-ray diffraction chamber for the study of a single crystal located in a polycrystalline sample</a> <b>[P]</b> . <span> 外国专利：  US3149228A </span> <span> . 1964-09-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：X射线衍射室，用于研究多晶样品中的单晶 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130490109779.html">X-RAY DIFFRACTION CHAMBER FOR THE STUDY OF A SINGLE CRYSTAL LOCATED IN A POLYCRYSTALLINE SAMPLE</a> <b>[P]</b> . <span> 外国专利：  CA700918A </span> <span> . 1964-12-29</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：X射线衍射腔，用于研究多晶样品中的单晶 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130490245461.html">X-ray diffraction chamber for the study of a single crystal located in a polycrystalline sample</a> <b>[P]</b> . <span> 外国专利：  GB955534A </span> <span> . 1964-04-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：X射线衍射室，用于研究多晶样品中的单晶 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 19px;z-index: 999;" onclick="ywcd('0704028161370','4',7,2,1,'',this,24)" class="delivery" prompt="010401" title="通过人工服务将文献原文发送至邮箱" >获取原文</div> <div class="journalsub-pop-up" style="display: none"> <div class="journal-sub"> <h2>期刊订阅</h2> <img src="https://cdn.zhangqiaokeyan.com/img/loginclose.png" alt="关闭" onclick="$('.journalsub-pop-up').hide()"> <p 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