Crystalline Boragermenes

Rao Bin; Kinjo Rei

摘要

Abstract > Boragermene 3 featuring a double bond between the Ge and dicoordinate B atoms has been synthesized for the first time by reacting the cyclic (alkyl)(boryl)germylene–PMe <sub>3</sub> adduct 1 with Cl <sub>2</sub> BN(SiMe <sub>3</sub> ) <sub>2</sub> followed by reductive dehalogenation with KC <sub>8</sub> . Addition of a Lewis base ( Me NHC) to 3 leads to the formation of the corresponding adduct 4 , which shows double bond character between the Ge and tricoordinate B atoms. Compound 3 undergoes hydrogenation with H <sub>2</sub> concomitant with a complete scission of the Ge=B bond. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 博尔加尔德 3 </ b> 通过使环状（烷基）（硼酸酯）常忍 - PME反应，首次合成Ge和Dicoorde B原子之间的双键。 <sub> 3 </ sub> 加合物 1 </ b> 用cl. <sub> 2 </ sub> BN（Sime. <sub> 3 </ sub> 的） <sub> 2 </ sub> 然后用KC减少脱卤 <sub> 8 </ sub> 。添加刘易斯基地（ me </ sup> nhc）到 3 </ b> 导致形成相应的加合物 4 </ b> ，在GE和三角B原子之间表示双键特性。化合物 3 </ b> 用h经历氢化 <sub> 2 </ sub> 伴随着GE = B键的完全裂变。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-19011/'>《Angewandte Chemie》</a> <b style="margin: 0 2px;">|</b><span>2020年第8期</span><b style="margin: 0 2px;">|</b><span>共4页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rao Bin&option=202" target="_blank" rel="nofollow">Rao Bin;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Kinjo Rei&option=202" target="_blank" rel="nofollow">Kinjo Rei;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Division of Chemistry and Biological ChemistryNanyang Technological UniversityNanyang Link 21 Singapore 637371 Singapore;</p> <p>Division of Chemistry and Biological ChemistryNanyang Technological UniversityNanyang Link 21 Singapore 637371 Singapore;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1188.html" title="应用化学">应用化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=boron&option=203" rel="nofollow">boron;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=double bonds&option=203" rel="nofollow">double bonds;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=germanium&option=203" rel="nofollow">germanium;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=H2 activation&option=203" rel="nofollow">H2 activation;</a> </p> <div class="translation"> 机译：硼;双键;锗;H2激活; 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