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首页> 外文期刊>Journal of mass spectrometry: JMS >Development of an extraction method for the quantification of lignans in espresso coffee by using HPLC‐MS/MS triple quadrupole
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Development of an extraction method for the quantification of lignans in espresso coffee by using HPLC‐MS/MS triple quadrupole

机译：用HPLC-MS / MS三重四极其促进浓缩咖啡中木质素的提取方法的开发

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Abstract > Lignans are polyphenolic compounds that are considered phytoestrogens for their plant origins, and they possess different biological activities. Three different extraction methods, ie, “dilute and shoot”, acidic hydrolysis, and enzymatic digestion, have been compared for extracting lignans (secoisolariciresinol (SECO), matairesinol (MAT), and lariciresinol (LARI)) from espresso coffee (EC) by using high‐performance liquid chromatography (HPLC) tandem mass spectrometry (MS/MS). The best recovery values (SECO: 97%, LARI: 98%, and MAT: 93%) were obtained by using enzymatic hydrolysis with Clara‐Diastase at 10% ( w / v ), keeping the sample at 37°C for 3?hours. For this reason, this method has been chosen and then applied to quantify lignans in 9 different EC samples from 5 different geographical origins (Brazil, Colombia, El Salvador, Ethiopia, and India). Secoisolariciresinol and LARI were found in all EC samples from 27.9 to 52.0?μg?L ?1 and from 5.3 to 27.8?μg?L ?1 respectively, contrary to MAT that it was not possible to detect it in each type of coffee. This method confirms the high specificity and sensitivity of MS/MS system for detecting bioactives in complex matrix such as coffee. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><abstract xmlns =“http://www.wiley.com/namespaces/wiley”type =“main”xml：lang =“en”> <title type =“main”>抽象</ title> > lignans是被认为是植物起源的多酚化合物，它们具有不同的生物活性。已经比较了从浓缩咖啡（EC）的浓缩咖啡（EC）中提取木质素（Secoisolaricirachol（Secoisolaricirsinol（Seco），MataIrsinol（Seco），Matairesinol（Seco），Lariciresinol（Lari））进行酸性水解和酶消化的三种不同的提取方法，即“稀释和芽”，酸性水解和酶消化。使用高效液相色谱（HPLC）串联质谱（MS / MS）。通过使用酶水解在10％（ W </ i> / v </ i>），将样品保持在37°C 3.小时。因此，已选择该方法，然后应用于从5种不同地理起源（巴西，哥伦比亚，萨尔瓦多，埃塞俄比亚和印度）的9种不同的EC样品中量化Lignans。在所有EC样品中发现SecoIsolariciresinol和Lari分别从27.9至52.0Ω·0≤μgΔ1 1和5.3〜27.8Ω·μgΔ1？1 </ sup>。相反，与垫子相反在每种类型的咖啡中都无法检测到它。该方法证实了MS / MS系统的高特异性和灵敏度，用于检测复杂矩阵中的生物术等咖啡。 </ p> </ abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-34906/'>《Journal of mass spectrometry: JMS》</a> <b style="margin: 0 2px;">|</b><span>2018年第9期</span><b style="margin: 0 2px;">|</b><span>共7页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Angeloni Simone&option=202" target="_blank" rel="nofollow">Angeloni Simone;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Navarini Luciano&option=202" target="_blank" rel="nofollow">Navarini Luciano;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Sagratini Gianni&option=202" target="_blank" rel="nofollow">Sagratini Gianni;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Torregiani Elisabetta&option=202" target="_blank" rel="nofollow">Torregiani Elisabetta;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Vittori Sauro&option=202" target="_blank" rel="nofollow">Vittori Sauro;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Caprioli Giovanni&option=202" target="_blank" rel="nofollow">Caprioli Giovanni;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>School of PharmacyUniversity of Camerinovia Sant’ Agostino 1 62032 Camerino Italy;</p> <p>illycaffè S.p.A.via Flavia 110 Trieste I‐34147 Italy;</p> <p>School of PharmacyUniversity of Camerinovia Sant’ Agostino 1 62032 Camerino Italy;</p> <p>School of PharmacyUniversity of Camerinovia Sant’ Agostino 1 62032 Camerino Italy;</p> <p>School of PharmacyUniversity of Camerinovia Sant’ Agostino 1 62032 Camerino Italy;</p> <p>School of PharmacyUniversity of Camerinovia Sant’ Agostino 1 62032 Camerino Italy;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1187.html" title="分析化学">分析化学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=espresso coffee&option=203" rel="nofollow">espresso coffee;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=HPLC‐MS/MS&option=203" rel="nofollow">HPLC‐MS/MS;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=lignans&option=203" rel="nofollow">lignans;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=polyphenols&option=203" rel="nofollow">polyphenols;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=SPE&option=203" rel="nofollow">SPE;</a> </p> <div class="translation"> 机译：浓咖啡;HPLC-MS / MS;木质素;多酚;SPE; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a 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