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Efficacy of uncommon surface treatment methods on titanium in order to improve bond strengths for adhesive cementation

机译:罕见的表面处理方法对钛的功效,以提高粘合剂胶结的结合强度

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摘要

The aim of this study is to comparison of effects of uncommon surface treatments, especially new alternatives on the adhesive strength between resin and titanium surfaces. Fifty-five titanium disks were prepared and they were separated into 5 groups as follows:(1) Control group; (2) Tribochemical treatment group in the laboratory; (3) Tribochemical treatment group in the clinic; (4) Acid etch group; and (5) Nd:YAG Laser-irradiated group. Surface roughness of the specimens was measured using a profilometer, and the topographic patterns were observed by scanning electron microscope. After these tests, resin cement was applied to the titanium samples. Shear bond test was performed via a universal testing machine at a crosshead speed of 0.5 mm/minute. In addition, the correlation between the surface roughness and bond strength was checked using Spearman correlation test (0.01 level). The highest surface roughness value was observed for the acid etch group (1.53 mu m). The highest mean shear bond strength was recorded with the tribochemical procedure group in the laboratory (13.74 MPa) and the lowest with the control group (3.69 MPa). A positive correlation was found between the bond strength and surface roughness for all groups. All of the surface treatment methods that were used in present study increased the bond strength between resin and titanium except for the laser group.
机译:这项研究的目的是比较罕见的表面处理效果,尤其是新的替代方法对树脂和钛表面之间的粘合强度的影响。制备55个钛盘,将它们分成5组,如下:(1)对照组; (2)实验室摩擦化学处理组; (3)诊所摩擦化学治疗组; (4)酸蚀基团; (5)Nd:YAG激光照射组。使用轮廓仪测量样品的表面粗糙度,并通过扫描电子显微镜观察其形貌图案。在这些测试之后,将树脂胶粘剂施加到钛样品上。通过万能试验机以0.5mm /分钟的十字头速度进行剪切粘结试验。另外,使用Spearman相关检验(0.01水平)检查了表面粗糙度和粘结强度之间的相关性。对于酸蚀刻组,观察到最高的表面粗糙度值(1.53μm)。摩擦化学程序组在实验室中记录的平均剪切粘结强度最高(13.74 MPa),而对照组则最低(3.69 MPa)。在所有组的粘结强度和表面粗糙度之间发现正相关。除激光组外,本研究中使用的所有表面处理方法均提高了树脂和钛之间的结合强度。

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