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Bond strength of veneering porcelain to zirconia after different surface treatments

机译:不同表面处理后饰面瓷与氧化锆的结合强度

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Aim: The aim of this study was to evaluate the effect of various surface treatments on the bond strength of veneering feldspathic porcelain to zirconia. Methods: Fifty yttria-stabilized tetragonal zirconia polycrystalline specimens were divided into five groups (n = 10) according to various surface treatments. The groups were as follows: Group 1: control group with liner application and no further surface treatment; Group 2: air-particle abrasion with 110 mu m of alumina (Al2O3) particles; Group 3: grinding with a diamond disk; Group 4: Nd:YAG laser irradiation (the laser and the energy parameters were 10 Hz, and 2 W and 200 mJ, and the pulse duration (short pulse) range was up to 180 mu s); Group 5: selective infiltration etching (SIE). After surface treatments, a liner application was performed for all surfaces according to the manufacturer's instructions. Veneering porcelain was applied on zirconia surfaces using a Teflon mold. Shear bond strength was tested using a universal testing machine. The fractured surface morphologies were examined with scanning electron microscopy. The data were statistically analyzed using Mann-Whitney U and Kruskal-Wallis tests (alpha = .05). Results: The Megapascal values of the bonding groups were as follows: G1 = 8.62 +/- 1.12, G2 = 13.87 +/- 5.08, G3 = 12.31 +/- 3.35, G4 = 17.32 +/- 6.16, and G5 = 16.17 +/- 4.55. Statistically significant differences were observed between the control group and the other groups (p < 0.05). Group 4 had the highest bond strength while G1 showed the lowest bond strength. No significant differences were found between the Nd: YAG, grinding, sandblasting, and SIE groups. Conclusion: Surface treatments had different effects on the shear bond strength of feldspathic porcelain to zirconia. Surface treatment techniques used in this study can be used on zirconia specimens prior to liner application to obtain an acceptable bond strength of veneering porcelain to zirconia. The effect of Nd: YAG laser irradiation and SIE techniques on bond strength of veneering ceramic to zirconia should be evaluated with further studies.
机译:目的:本研究的目的是评估各种表面处理对贴面长石瓷与氧化锆结合强度的影响。方法:根据不同的表面处理方法,将50个氧化钇稳定的四方氧化锆多晶样品分为5组(n = 10)。各组如下:第1组:对照组,有衬纸施用,没有进一步的表面处理;第2组:用110微米的氧化铝(Al2O3)颗粒进行空气颗粒磨损;第三组:用金刚石盘磨;第4组:Nd:YAG激光照射(激光和能量参数分别为10 Hz,2 W和200 mJ,脉冲持续时间(短脉冲)范围高达180μs);第5组:选择性渗透蚀刻(SIE)。表面处理后,根据制造商的说明对所有表面进行衬板施工。使用特氟龙模具将饰面瓷涂在氧化锆表面上。剪切粘结强度使用通用测试机进行测试。用扫描电子显微镜检查断裂的表面形态。使用Mann-Whitney U和Kruskal-Wallis检验对数据进行统计分析(α= 0.05)。结果:键合基团的兆帕值如下:G1 = 8.62 +/- 1.12,G2 = 13.87 +/- 5.08,G3 = 12.31 +/- 3.35,G4 = 17.32 +/- 6.16,G5 = 16.17 + /-4.55。在对照组和其他组之间观察到统计学上的显着差异(p <0.05)。第4组的粘结强度最高,而G1的粘结强度最低。 Nd:YAG,研磨,喷砂和SIE组之间没有发现显着差异。结论:表面处理对长石瓷与氧化锆的剪切粘结强度有不同的影响。本研究中使用的表面处理技术可以在衬里应用之前用于氧化锆样品,以获得饰面瓷与氧化锆的可接受的粘结强度。 Nd:YAG激光辐照和SIE技术对饰面陶瓷与氧化锆结合强度的影响应进行进一步研究。

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