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Optimization of processing parameters for graphitization of oil palm trunk waste at lower heating temperature

机译:较低加热温度下油棕榈树干浪费石墨化处理参数的优化

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Previously synthetic graphite was produced at higher temperature which is around 2,500 °C in complex processing method. The method bear the name of the scientist whose discover the synthetic graphite namely "Acheson Process". However, via pyrolysis process, in controlled heating condition, and specific heating rate by utilizing oil palm trunk waste, synthetic graphite was managed to produce at much lower heating temperature. In this research, the heating temperature were varied in the range of 500 °C, 800 °C, and 1,000 °C. The heating rate applied also varied, from 5 °/min to 10 °/min and 20 °/min. After heating treatment, the samples were characterized using X-ray Diffraction (XRD) and analysed by X'Pert Highscore Plus software. Graphitic nature of the synthetic graphite produced was further supported by RAMAN analysis. The morphological study was carried out by using Scanning Electron Microscope (SEM). Based on the analysis, optimum processing parameters was optimized. It is at the temperature of 800 °C and at the heating rate of 20 °/min.
机译:以前在较高温度下生产的合成石墨在复杂的加工方法中为约2,500℃。该方法承载科学家的名称,其发现合成石墨即“Acheson Process”。然而,通过热解过程,通过利用油棕树干浪费,通过利用油棕榈树干废物来制造合成石墨,加热温度低得多。在该研究中,加热温度在500℃,800℃和1,000℃的范围内变化。施加的加热速率也变化,5°/ min至10°/ min和20°/ min。在加热处理后,使用X射线衍射(XRD)表征样品,并由X'Pert HighScore加软件分析。通过拉曼分析进一步支持产生的合成石墨的石墨性质。通过使用扫描电子显微镜(SEM)进行形态学研究。基于分析,优化了最佳处理参数。它处于800℃的温度,加热速率为20°/ min。

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