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Preparation of porous carbon with zinc oxide template

机译:氧化锌模板多孔碳的制备

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摘要

The porous carbon materials were prepared by the following processes of evaporation induction self-assembly (EISA), thermal polymerization process and calcination step at high temperature with the nano-zinc oxide as a hard template and phenol resin as carbon source. The as-prepared porous carbon materials were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), N_2 adsorption/desorption isotherms (BET) and Fourier transform infrared spectroscopy (FT-IR). The adsorption performance was investigated via removal ciprofloxacin antibiotic. The results showed that the more the amount of zinc oxide template was added in the prepared process of porous carbon, the clearer pore channel of as-prepared porous carbon was exhibited. When the dosage of zinc oxide reach 0.4 g, it is well formed a preferably porous carbon, the higher adsorption rate of ciprofloxacin with 100 mL of 15 mg/L could reach 71.2%.
机译:通过以下用纳米氧化锌作为硬模板和酚醛树脂作为碳源,通过以下蒸发感应自组装(EISA),热聚合方法和煅烧步骤的方法,热聚合方法和煅烧步骤制备多孔碳材料。通过扫描电子显微镜(SEM),透射电子显微镜(TEM),N_2吸附/解吸等温线(BET)和傅里叶变换红外光谱(FT-IR),以制备的多孔碳材料表征。通过去除环丙沙星抗生素研究吸附性能。结果表明,在多孔碳的制备过程中加入氧化锌模板的量越多,所制备的多孔碳的更清晰的孔通道。当氧化锌的剂量达到0.4g时,它形成优选多孔碳,环丙沙星的较高吸附速率,100ml 15mg / L可以达到71.2%。

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