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The preparation of oriented samples of ferromagnetic shape memory alloy CoNiAl

机译:制备铁磁形状记忆合金圆锥定向样品

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摘要

In the present study, the set of the directionally solidified samples from alloy with the nominal composition Co_(38)Ni_(33)Al_(29) were prepared using the Bridgman and the floating zone method. Various growth rates results in various solidification structures, mainly different ratio of the disordered phase γ-cobalt solid solution and the ordered phase β-B2 (Co.Ni)Al. The ratio has the fundamental effect on the temperature of the martensitic phase transition. This evolution of the samples structure was studied by metallography, SEM, EPMA and EBSD methods. The results are discussed in the frame of decomposition kinetics of this ternary alloy. The samples without high-angle grain boundaries, i.e., single-crystals, can be cut from the prepared directional grown ingots and used to examine mechanical properties.
机译:在本研究中,使用Bridgman和浮区法制备来自具有标称组合物CO_(38)Ni_(39)的合金的定向固化的样品。各种生长速率导致各种凝固结构,主要是无序相γ-钴固溶和有序相β-B2(Co.I)的不同比例。该比率对马氏体相转变的温度具有根本影响。通过金相,SEM,EPMA和EBSD方法研究了样品结构的这种演变。该结果在该三元合金的分解动力学框架中讨论。没有高角度晶界,即单晶的样品可以从制备的定向生长的锭切割并用于检查机械性能。

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