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Influence of Technological Conditions on the Properties of PcBN Composites Fabricated by Spark Plasma Sintering

机译:工艺条件对火花等离子体烧结制备PcBN复合材料性能的影响

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Polycrystalline cubic boron nitride (PcBN) composites were fabricated by spark plasma sintering (SPS). The SiC, Si_3N_4 and Si/B were used as binder. The effects of SPS sintering process parameters, such as the sintering temperature, holding time, heating rate and binder composition, on the properties of PcBN samples were investigated. PcBN composite with a hardness of 23.12GPa was fabricated efficiently by SPS. The hardness of PcBN sample increased first and then decreased with the increase of sintering temperature. As the holding time was 20 min, the hardness of PcBN sample was the highest. The PcBN performance at the heating rate of 50 °C/min was significantly better than that of 100°C /min. When the binder component of SiC, Si_3N_4, and Si was 63%:27%:10%, the hardness of PcBN was the highest. With an addition of Si, the PcBN samples had higher hardness than that of B.
机译:通过火花等离子体烧结(SPS)制备了多晶立方氮化硼(PcBN)复合材料。 SiC,Si_3N_4和Si / B用作粘合剂。研究了烧结温度,保温时间,加热速率和粘结剂组成等SPS烧结工艺参数对PcBN样品性能的影响。用SPS有效地制备了硬度为23.12GPa的PcBN复合材料。随着烧结温度的升高,PcBN样品的硬度先升高后降低。由于保持时间为20分钟,因此PcBN样品的硬度最高。加热速率为50°C / min时,PcBN性能明显优于100°C / min。当SiC,Si_3N_4和Si的粘合剂成分为63%:27%:10%时,PcBN的硬度最高。加入Si后,PcBN样品的硬度高于B。

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