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Method for producing separation membrane using MFI-type zeolite (silicalite)

机译:使用MFI型沸石(硅沸石)制备分离膜的方法

摘要

Provided is a method for producing a separation membrane including a silicalite membrane without using NaOH or the like that causes an increase in cost with respect to equipment, facilities, and process time. The method for producing a separation membrane is a method for producing a separation membrane including a porous support and a silicalite membrane that is formed on the support and has an MFI-type zeolite crystal structure, and is characterized in that the method includes a step of producing a seed crystal, a step of attaching the seed crystal onto the porous support, a step of producing a membrane synthesis raw material composition containing SiO2, an organic template, and H2O, and a step of immersing the porous support having the seed crystal attached thereto in the membrane synthesis raw material composition and performing hydrothermal synthesis, and the composition ratio of the membrane synthesis raw material composition is as follows: SiO2:organic template:H2O=1:(0.05 to 0.15):(50 to 120).
机译:提供了一种用于制造包括硅膜的分离膜的方法,而不使用NaOH等,这导致设备,设施和处理时间增加成本。用于制备分离膜的方法是制备具有多孔载体和形成在载体上的硅膜和具有MFI型沸石晶体结构的分离膜的方法,其特征在于该方法包括步骤产生晶种,将籽晶与多孔载体附着的步骤,其制造含有SiO 2,有机模板和H 2 O的膜合成原料组合物的步骤,以及浸入具有所连接的种子晶体的多孔载体的步骤其在膜合成原料组合物中并进行水热合成,膜合成原料组合物的组成比如下:SiO2:有机模板:H 2 O = 1:(0.05至0.15):( 50至120)。

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