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Device for separation of sputtered neutrals and high energy ions from sputtered low energy ions

机译:用于将溅射的中性离子和高能离子与溅射的低能离子分离的装置

摘要

A device capable of reducing the background in ion probe mass spectrometry by up to seven orders of magnitude (107) allows separation of sputtered neutrals and high energy sputtered or backscattered ions from low energy sputtered ions. The low energy sputtered ions are fed into a mass analyzer for determination of the mass-to-charge ratio whereas the neutrals and high energy ions which usually produce a high background intensity in the mass spectra are prevented from entering the mass analyzer. This is achieved by positioning the target off-axis with respect to the relevant analyzer axis on the entrance side of the mass analyzer, by placing a shutter with an aperture between target and entrance aperture of the mass analyzer so that sputtered neutrals passing through the shutter aperture impinge on the front panel of the mass analyzer outside the entrance aperture, by producing an electric field between shutter and front panel of the mass analyzer, and by adjusting the direction and strength of the electric field in such a way that low energy sputtered ions passing through the shutter aperture can be deflected into the entrance aperture of the mass analyzer whereas high energy ions are less deflected and thus impinge on the front panel of the mass analyzer outside the entrance aperture.
机译:一种能够将离子探针质谱分析中的背景降低多达七个数量级的设备(107),可将溅射的中性离子和高能溅射或背散射离子与低能溅射离子分离。将低能溅射离子送入质量分析仪中,以测定质荷比,而通常会在质谱图中产生高背景强度的中性离子和高能离子则无法进入质量分析仪。这是通过以下方式实现的:将目标偏轴相对于质量分析仪入口侧的相关分析仪轴定位,通过在光阑和质量分析仪的入口孔径之间放置一个孔径小的百叶窗,使溅射出的中性粒子穿过百叶窗通过在百叶窗和质量分析仪的前面板之间产生电场,并通过调节电场的方向和强度以使低能溅射离子进入电子束孔,从而在入射孔外部撞击质量分析仪的前面板穿过百叶窗光阑的光束可以偏转到质量分析仪的入口孔中,而高能离子偏转较少,因此会撞击到质量分析仪的前面板入口孔之外。

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