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Method of preparation of the sodium benzoate by catalytic oxidation of the toluene in the liquid phase

机译:通过液相催化甲苯氧化制备苯甲酸钠的方法

摘要

P according to the invention, benzoic acid obtained is treated hot with a small amount of amine of formula r n - h2 in which r represents hydrogen, an alkyl or cycloalkyl c1 - c4, c5 - c6, or a salt of such an amine, simultaneously or thereafter, to a distillation or a sublimation of a manner known per se, is then reacted with soda lye and is treated by extraction with toluene and / or by steam distillation of water in a manner known in the ground and / p & & p & sodium benzoate obtained according to the invention meets the requirements of the pharmacopoeiae of the main nations. / p
机译:

根据本发明,将得到的苯甲酸用少量的式rn-h2的胺进行热处理,其中r代表氢,烷基或环烷基的c1-c4,c5-c6或此类胺的盐同时或之后,以本身已知的方式进行蒸馏或升华,然后与纯碱反应,并通过用甲苯萃取和/或通过水蒸气蒸馏的方式以地面已知的方式进行处理, & & &根据本发明获得的苯甲酸钠满足主要国家药典的要求。

著录项

  • 公开/公告号FR2361331A1

    专利类型

  • 公开/公告日1978-03-10

    原文格式PDF

  • 申请/专利权人 BAYER AG;BAYER AG;

    申请/专利号FR19770024956

  • 发明设计人

    申请日1977-08-12

  • 分类号C07C63/08;C07C51/42;

  • 国家 FR

  • 入库时间 2022-08-22 21:45:24

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