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PROCESS FOR THE PREPARATION OF GUAIACOL GLYCERYL ETHER

机译:愈创木酚甘油醚的制备方法

摘要

Guaiacol glycerine ether is obtained in very good yield and in very high purity by reacting glycidol with o-methyoxyphenol in the presence of an alkali hydroxide, an alkali alcoholate, an alkali cyanate or an alkali thiocyanate at 80 DEG to 150 DEG C. An especially effective purification of the crude product can be obtained by adding hydrogen peroxide, preferably prior to cooling.
机译:通过在80至150℃下在碱金属氢氧化物,碱金属醇盐,碱金属氰酸盐或碱金属硫氰酸盐的存在下使缩水甘油与邻甲氧基苯酚反应,以非常高的产率和非常高的纯度获得了愈创木酚甘油醚。有效地提纯粗产物可以通过添加过氧化氢来获得,优选在冷却之前。

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