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QUALITATIVE AND QUANTITATIVE ANALYZER FOR THIN LAYERED CHROMATOGRAPHY

机译:薄层色谱的定性和定量分析仪

摘要

PURPOSE:To enable direct qualitative and quantitative analysis, by incorporating a chromatographic spectrophotometer performing the quantitative analysis of each single component and a photoacoustic analysis performing the analysis of each single component by utilizing photoacoustic effect in the same apparatus. CONSTITUTION:White light is emitted to a first light path A from a white light source 4 and converted to monochromatic light by a spectroscope 5 to irradiate the thin layered chromatographic plate in a measuring cell 1. The reflected light from the thin layered chromatographic plate is guided to a detector 9 and quantified data is obtained by a specific measuring device 10. This quantified data is stored in a memory 34 through LPF32 and an A/D converter 33. A computer 31 drives a pulse motor 3 to allow a second light path B to coincide with the position corresponding to the peak value of the quantified value data. Infrared rays are emitted to the light path B from an infrared source 21 to be guided to the cell 1. The microphone 26 provided to the cell 1 detects the pressure wave generated by infrared rays as a sonic wave. This detection signal is inputted to a Fourier transformation apparatus 28 to obtain the qualitative data of each unit component.
机译:目的:为了实现直接的定性和定量分析,通过在同一装置中结合使用色谱分光光度计对每个单一组分进行定量分析和对光声分析进行分析,利用光声效应对每个单个组分进行分析。组成:白光从白光源4发射到第一光路A,并由分光镜5转换为单色光,以照射测量单元1中的薄层色谱板。薄层色谱板的反射光为被引导至检测器9的信号,并由特定的测量设备10获得量化的数据。该量化的数据通过LPF32和​​A / D转换器33存储在存储器34中。计算机31驱动脉冲电动机3以允许第二光路B与与量化数据的峰值对应的位置一致。红外线从红外线源21发射到光路B,并被引导至单元格1。设置在单元格1中的麦克风26将由红外线产生的压力波检测为声波。该检测信号被输入到傅立叶变换装置28,以获得每个单位分量的定性数据。

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